Change search
CiteExportLink to record
Permanent link

Direct link
Cite
Citation style
  • apa
  • ieee
  • modern-language-association-8th-edition
  • vancouver
  • Other style
More styles
Language
  • de-DE
  • en-GB
  • en-US
  • fi-FI
  • nn-NO
  • nn-NB
  • sv-SE
  • Other locale
More languages
Output format
  • html
  • text
  • asciidoc
  • rtf
Defects in E-PBF Ti-6Al-4V and their Effect on Fatigue Behaviour: Characteristics, Distribution and Impact on Life
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Material Science.ORCID iD: 0000-0003-3828-2149
2020 (English)Licentiate thesis, comprehensive summary (Other academic)Alternative title
Defekter i E-PBF Ti-6Al-4V och dess effekter på utmattningsegenskaper : Kännetecken, fördelning och livslängdspåverkan (Swedish)
Abstract [en]

Layer by layer manufacturing (additive manufacturing, AM) of metals is emerging as an alternative to conventional subtractive manufacturing with the goal of enabling near net-shape production of complex part geometries with reduced material waste and shorter lead times. Recently this field has experienced rapid growth through industrial adaptation but has simultaneously encountered challenges. One such challenge is the ability of AM metal to withstand loading conditions ranging from static loads to complex multiaxial thermo-mechanical fatigue loads. This makes fatigue performance of AM materials a key consideration for the implementation of AM in production. This is especially true for AM in the aerospace industry where safety standards are strict.

Defects in metal AM materials include rough surfaces, pores and lack-of-fusion (LOF) between build layers. These defects are detrimental to fatigue as they act as local stress concentrators that can give rise to cracks in the material.  Some defects can be avoided by careful build process optimization and/or post-processing but fully eliminating all defects is not possible. Because of this, a need arises for the capability to estimate the fatigue performance of AM produced critical components containing defects.

The aim of the thesis is to increase understanding regarding the connection between defect characteristics and the fatigue behaviour in AM produced Ti-6Al-4V. Defect distributions are statistically analysed for use in a simple fracture mechanical model for fatigue life prediction. Other study areas include the impact of post-production treatments such as chemical surface treatments and hot isostatic pressing (HIP) on defects and fatigue behaviour.

The thesis constitutes three scientific papers. The AM technique studied in these papers is Electron Beam Melting (EBM) in which an electron beam selectively melts pre-alloyed metal powder. In paper 1, defects were studied using X-ray computed tomography (XCT) and fatigue crack initiation was related to the observed defect distribution. In paper 2, XCT data was used to relate the surface morphology and roughness of post-production treated EBM material to the surface near defect distribution. The connection between this distribution and manufacturing parameter has also been explored. Paper 3 builds on and extends the work presented in paper 1 by including further fatigue testing as well as a method for predicting fatigue life using statistical analysis of the observed defect distribution.

The impact of a defect on the fatigue behaviour of the material was found to largely depend on its characteristics and position relative to the surface. Production and post-processing of the material was found to play a role in the severity of this impact. Finally, it was found that a probabilistic statistical analysis can be used to accurately predict the life of the studied material at the tested conditions.

Place, publisher, year, edition, pages
Luleå: Luleå tekniska universitet, 2020.
Series
Licentiate thesis / Luleå University of Technology, ISSN 1402-1757
Keywords [en]
Defects, Additive Manufacturing, Ti-6Al-4V, Probabilistic Modelling, Fatigue
National Category
Metallurgy and Metallic Materials
Research subject
Engineering Materials
Identifiers
URN: urn:nbn:se:ltu:diva-81155ISBN: 978-91-7790-685-8 (print)ISBN: 978-91-7790-686-5 (electronic)OAI: oai:DiVA.org:ltu-81155DiVA, id: diva2:1476877
Presentation
2020-12-10, E632, Luleå, 09:30 (English)
Opponent
Supervisors
Projects
SUDDENAvailable from: 2020-10-16 Created: 2020-10-15 Last updated: 2024-10-24Bibliographically approved
List of papers
1. X-ray Micro Tomography Study of Internal Defects of Electron Beam Melted Ti6Al4V and Their Effect on Fatigue Behavior
Open this publication in new window or tab >>X-ray Micro Tomography Study of Internal Defects of Electron Beam Melted Ti6Al4V and Their Effect on Fatigue Behavior
Show others...
2020 (English)In: / [ed] P. Villechaise, B. Appolaire, P. Castany, M. Dehmas, C. Delaunay, J. Delfosse, A. Denquin, E. Gautier, L. Germain, N. Gey, T. Gloriant, J.-Y. Hascoët, S. Hémery, Y. Millet, D. Monceau, F. Pettinari-Sturmel, M. Piellard, F. Prima and B. Viguier, EDP Sciences, 2020, article id 03029Conference paper, Published paper (Refereed)
Abstract [en]

In this work, the fatigue behaviour of Ti6Al4V manufactured using electron beam melting, its dependency on porosity, distance from the base plate and build layer height were investigated. XCT scans of the fatigue sample gauge lengths were correlated to SEM investigations of the fracture surfaces. A comparison between the top and bottom halves of the builds in terms of defect population and fatigue behaviour was also made. Larger pores were detected in samples with a larger build layer height and lower position in the build chamber. Results also indicate that part geometry and pore location, specifically closeness to the surface, are important factors regarding the initiation location of fatigue fractures at 1 % strain. Furthermore, a fatigue critical lack of fusion defect was undetectable in the XCT scan.

Place, publisher, year, edition, pages
EDP Sciences, 2020
Series
MATEC Web of Conferences, E-ISSN 2261-236X ; 321
National Category
Other Materials Engineering Fluid Mechanics Applied Mechanics
Research subject
Engineering Materials; Fluid Mechanics; Experimental Mechanics
Identifiers
urn:nbn:se:ltu:diva-81150 (URN)10.1051/matecconf/202032103029 (DOI)
Conference
14th World Conference on Titanium (Ti 2019), 10-14 June, 2019, Nantes, France
Projects
SUDDEN
Funder
Vinnova, 2017-04846
Available from: 2020-10-15 Created: 2020-10-15 Last updated: 2025-02-09Bibliographically approved
2. Effect of chemical post-processing on surfaces and sub-surface defects in electron beam melted Ti-6Al-4V
Open this publication in new window or tab >>Effect of chemical post-processing on surfaces and sub-surface defects in electron beam melted Ti-6Al-4V
Show others...
2022 (English)In: Materials Characterization, ISSN 1044-5803, E-ISSN 1873-4189, Vol. 193, article id 112281Article in journal (Refereed) Published
Abstract [en]

Surfaces after chemical post-processing treatments of electron beam melting (EBM) produced Ti-6Al-4V have been studied. Targeted chemical treatment allowed the study of variation in surface quality with material removal depth. Characterization of surface and defect morphologies were made, comparing two chemical post-processing methods, Hirtisation® and chemical milling with different milling depths. Surface topography was characterized using white light interferometry and subsurface defect distribution was studied using X-ray computed tomography (XCT). The morphology of the surface at different milling depths was compared to the sub-surface information from XCT scans of the as-built material. Furthermore, Hot Isostatic Pressing (HIP) treated material was documented for comparison. Results show that post-processed surfaces contain a number of different defects of mixed morphology, position and origin. Post-processing deteriorates the surface quality with increased removal depth due to the presence of sub-surface defects. The position of sub-surface defects in relation to the material surface coincides with the depth at which contour-hatch interactions are likely to have occurred during the EBM building process. The distribution of this sub-surface defect population is anisotropic in the building (horizontal) plane and reasons for this are explored. Hirtisation® produces surfaces morphologically different from chemically milled surfaces. This difference was found to contribute to Hirtisation® producing surfaces with higher roughness (Sa) than chemically milled surfaces at comparable removal depth. HIP did remove all detectable sub-surface defects but microstructural artefacts indicating healed porosity were found.

Place, publisher, year, edition, pages
Elsevier, 2022
Keywords
Electron beam melting, Chemical post-processing, Defects, X-ray computed tomography, Surface roughness
National Category
Metallurgy and Metallic Materials
Research subject
Engineering Materials
Identifiers
urn:nbn:se:ltu:diva-81153 (URN)10.1016/j.matchar.2022.112281 (DOI)000862845800001 ()2-s2.0-85138088971 (Scopus ID)
Projects
SUDDEN
Funder
Vinnova, 2017–04846
Note

Validerad;2022;Nivå 2;2022-09-26 (joosat);

Funder: GKN Aerospace Sweden AB

This article has previously appeared as a manuscript in a thesis.

Available from: 2020-10-15 Created: 2020-10-15 Last updated: 2023-09-05Bibliographically approved
3. Defects in Electron Beam Melted Ti-6Al-4V: Fatigue Life Prediction Using Experimental Data and Extreme Value Statistics
Open this publication in new window or tab >>Defects in Electron Beam Melted Ti-6Al-4V: Fatigue Life Prediction Using Experimental Data and Extreme Value Statistics
Show others...
2021 (English)In: Materials, E-ISSN 1996-1944, Vol. 14, no 3, article id 640Article in journal (Refereed) Published
Abstract [en]

Electron beam melting is a powder bed fusion (PBF) additive manufacturing (AM) method for metals offering opportunities for the reduction of material waste and freedom of design, but unfortunately also suffering from material defects from production. The stochastic nature of defect formation leads to a scatter in the fatigue performance of the material, preventing wider use of this production method for fatigue critical components. In this work, fatigue test data from electron beam melted Ti-6Al-4V specimens machined from as-built material are compared to deterministic fatigue crack growth calculations and probabilistically modeled fatigue life. X-ray computed tomography (XCT) data evaluated using extreme value statistics are used as the model input. Results show that the probabilistic model is able to provide a good conservative life estimate, as well as accurate predictive scatter bands. It is also shown that the use of XCT-data as the model input is feasible, requiring little investigated material volume for model calibration.

Place, publisher, year, edition, pages
MDPI, 2021
Keywords
additive manufacturing, electron beam melting, Ti-6Al-4V, defects, fatigue life, fracture mechanics, fatigue crack propagation, probabilistic modeling
National Category
Other Materials Engineering
Research subject
Engineering Materials
Identifiers
urn:nbn:se:ltu:diva-81154 (URN)10.3390/ma14030640 (DOI)000615396300001 ()33573246 (PubMedID)2-s2.0-85100309316 (Scopus ID)
Projects
SUDDEN
Funder
Vinnova, 2017-04846
Note

Validerad;2021;Nivå 2;2021-02-16 (alebob);

Artikeln har tidigare förekommit som manuskript i avhandling

Available from: 2020-10-15 Created: 2020-10-15 Last updated: 2024-07-04Bibliographically approved

Open Access in DiVA

fulltext(19267 kB)895 downloads
File information
File name FULLTEXT01.pdfFile size 19267 kBChecksum SHA-512
f03b894936f8cc970b89b1480d73270a5f26054f41f564a63047cd14c26883ba36a43099378a3f19a4e3ef56b6455070f291bb4ecbad6560fe8311de6832ad58
Type fulltextMimetype application/pdf

Authority records

Sandell, Viktor

Search in DiVA

By author/editor
Sandell, Viktor
By organisation
Material Science
Metallurgy and Metallic Materials

Search outside of DiVA

GoogleGoogle Scholar
Total: 2053 downloads
The number of downloads is the sum of all downloads of full texts. It may include eg previous versions that are now no longer available

isbn
urn-nbn

Altmetric score

isbn
urn-nbn
Total: 1253 hits
CiteExportLink to record
Permanent link

Direct link
Cite
Citation style
  • apa
  • ieee
  • modern-language-association-8th-edition
  • vancouver
  • Other style
More styles
Language
  • de-DE
  • en-GB
  • en-US
  • fi-FI
  • nn-NO
  • nn-NB
  • sv-SE
  • Other locale
More languages
Output format
  • html
  • text
  • asciidoc
  • rtf