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Multi-elemental characterization of soft biological tissues by inductively coupled plasma-sector field mass spectrometry
Luleå tekniska universitet.
ALS Analytica AB, Luleå.
ALS Analytica AB, Luleå.
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2004 (English)In: Analytica Chimica Acta, ISSN 0003-2670, E-ISSN 1873-4324, Vol. 521, no 2, p. 123-135Article in journal (Refereed) Published
Abstract [en]

The performance of double-focusing, sector field ICP-MS (ICP-SFMS) for the multi-elmental analysis of soft tissues following microwave-assisted digestion with nitric acid was eveluated and factors affecting method limits of detection discussed. Accuracy was assessed by replicate analyses of certified reference materials and by participation in performance evaluation programs; the precision was better than 5% relative standard deviation (RSD) for the majority of elements. Cl was the only element for which ICP-SFMS data consistently deviated from certified concentrations in the reference materials tested. Comparison between results obtained by ICP-SFMS and ICP optical emission spectrometry showed good agreement for elements present in tissues at concentrations above 2 μg g-1. The concentrations of 68 elements in different fish and animal soft tissues (muscle, liver, kidney, lung and brain) are presented, and, where possible, compared to previously published data.

Place, publisher, year, edition, pages
2004. Vol. 521, no 2, p. 123-135
National Category
Geochemistry
Research subject
Applied Geology
Identifiers
URN: urn:nbn:se:ltu:diva-8939DOI: 10.1016/j.aca.2004.06.030ISI: 000223611500002Scopus ID: 2-s2.0-4143073621Local ID: 77de7190-7581-11dc-824d-000ea68e967bOAI: oai:DiVA.org:ltu-8939DiVA, id: diva2:981877
Note
Validerad; 2004; 20071008 (emmeng)Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2018-07-10Bibliographically approved

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Engström, EmmaBaxter, DouglasRodushkin, Ilya

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