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Coherence transfer signals in the rotational resonance NMR of a spinning single crystal
Luleå University of Technology, Department of Civil, Environmental and Natural Resources Engineering, Sustainable Process Engineering.ORCID iD: 0000-0003-1067-7990
Stockholm University.
2000 (English)In: Journal of magnetic resonance, ISSN 1090-7807, E-ISSN 1096-0856, Vol. 147, no 1, p. 147-151Article in journal (Refereed) Published
Abstract [en]

A recent analysis of rotational resonance lineshapes (M. Helmle et al., J. Magn. Reson. 140, 379-403, 1999) predicted the existence of coherence transfer signals, which are generated by mechanically induced coherence transfer during the detection process. These signals correspond to the generation of observable coherences at spin sites that have no magnetization at the beginning of the observation interval but which acquire coherence while the detection is underway. The coherence transfer signals disappear for powder samples in conventional magic-angle-spinning solid-state NMR experiments. In this Communication, we report the successful detection of coherence transfer signals in rotor-synchronized experiments performed on a single crystal of [1,2-13C2]glycine.

Place, publisher, year, edition, pages
2000. Vol. 147, no 1, p. 147-151
National Category
Physical Chemistry
Research subject
Chemistry of Interfaces
Identifiers
URN: urn:nbn:se:ltu:diva-10753DOI: 10.1006/jmre.2000.2169ISI: 000165204800018Local ID: 99bb1810-bc07-11db-a46c-000ea68e967bOAI: oai:DiVA.org:ltu-10753DiVA, id: diva2:983700
Note

Validerad; 2000; 20070214 (bajo)

Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2018-07-10Bibliographically approved

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Antzutkin, Oleg

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