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Noninvasive in situ identification and band assignments of some pharmaceutical excipients inside USP vials with FT-near-infrared spectroscopy
Chemical and Forensic Sciences, School of Life Sciences, University of Bradford.
Chemical and Forensic Sciences, School of Life Sciences, University of Bradford.
2009 (engelsk)Inngår i: Spectrochimica Acta Part A - Molecular and Biomolecular Spectroscopy, ISSN 1386-1425, E-ISSN 1873-3557, Vol. 72, nr 4, s. 890-896Artikkel i tidsskrift (Fagfellevurdert) Published
Abstract [en]

For the manufacture of dosage forms all ingredients must be reliably identified. In this paper, the suitability of FT-NIR spectroscopy to identify potassium sorbate, sodium starch glycollate, calcium ascorbate, calcium carbonate, candelilla wax, maltosextrin, monohydrated and anhydrous lactose inside USP vials was investigated. Differentiation between the anhydrous and monohydrated forms of lactose was found to be possible by studying the regions of the near-infrared spectrum corresponding to the combination and first overtone stretching frequencies of water. The results show unequivocally the potential of FT-NIR spectroscopy for rapid, in situ and non-destructive identification of pharmaceutical excipients

sted, utgiver, år, opplag, sider
2009. Vol. 72, nr 4, s. 890-896
Identifikatorer
URN: urn:nbn:se:ltu:diva-11533DOI: 10.1016/j.saa.2008.12.010Lokal ID: a88d6670-e342-11df-8b36-000ea68e967bOAI: oai:DiVA.org:ltu-11533DiVA, id: diva2:984483
Merknad
Upprättat; 2009; 20101029 (andbra)Tilgjengelig fra: 2016-09-29 Laget: 2016-09-29 Sist oppdatert: 2017-11-24bibliografisk kontrollert

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