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PZT phase formation monitored by high-temperature X-ray diffractometry
Luleå tekniska universitet.
École Polytechnique Fédérale de Lausanne.
École Polytechnique Fédérale de Lausanne.
1997 (English)In: Journal of the European Ceramic Society, ISSN 0955-2219, E-ISSN 1873-619X, Vol. 17, no 6, p. 813-818Article in journal (Refereed) Published
Abstract [en]

The crystallisation kinetics of amorphous sol-gel PZT thin films were investigated using high-temperature X-ray diffraction. Crystallisation for different isotherms was monitored as a function of time. Phase transformation data were obtained from integrated X-ray peak intensities which were calibrated based on image analysis of the surface microstructure of the samples at the end of the isothermal treatments. An activation energy of 310 kJ/mol was obtained without assuming a specific kinetic model. From the transformation data, a TTT diagram was constructed for the ranges studied.

Place, publisher, year, edition, pages
1997. Vol. 17, no 6, p. 813-818
National Category
Other Materials Engineering
Research subject
Engineering Materials
Identifiers
URN: urn:nbn:se:ltu:diva-14544DOI: 10.1016/S0955-2219(96)00133-1ISI: A1997WQ72500009Local ID: deaca750-f3ec-11db-ac9f-000ea68e967bOAI: oai:DiVA.org:ltu-14544DiVA, id: diva2:987517
Note
Godkänd; 1997; 20070426 (cira)Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2018-07-10Bibliographically approved

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