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Simple directed material design through in situ substitution of proton with Cu+ ions
Institute of Chemistry and Chemical Engineering, University of Jinan, No.106, Jiwei Road, 250022, Jinan, Shandong, People’s Republic of China.
Institute of Chemistry and Chemical Engineering, University of Jinan, No.106, Jiwei Road, 250022, Jinan, Shandong, People’s Republic of China.
Institute of Chemistry and Chemical Engineering, University of Jinan, No.106, Jiwei Road, 250022, Jinan, Shandong, People’s Republic of China.
Luleå tekniska universitet, Institutionen för samhällsbyggnad och naturresurser, Industriell miljö- och processteknik.ORCID-id: 0000-0001-9794-8305
2009 (engelsk)Inngår i: Journal of Inorganic and Organometallic Polymers and Materials, ISSN 1574-1443, Vol. 19, nr 4, s. 485-493Artikkel i tidsskrift (Fagfellevurdert) Published
Abstract [en]

A new inorganic-organic hybrid material (C10H8N2H)2(Mo8O26) · 2NH4 (1) was prepared under solvothermal conditions (H2O/ethanol), which was then used as a starting material in the synthesis of another material, (C10H8N2Cu)2(Mo8O26) · 2NH4 (2). Each compound has been characterized by single-crystal X-ray diffraction, X-ray powder diffraction, elemental analysis, thermogravimetric analysis, fluorescence, FT-IR, and bond valence sum calculations. The comparative study focuses on the transformation and structural change between 1 and 2, which arises from the simple substitution of the proton in 1 with the Cu+ ions. The other surprising feature is that Cu+ ions can not only directly be used to substitute the proton of 1 but also ameliorate its photoluminescence property. It means that 1 appears to have recognizable functional protons in the solid-state structure and, hence, can very well be considered as an ideal precursor agent to design the functional materials with special architectures and photoactive properties.

sted, utgiver, år, opplag, sider
2009. Vol. 19, nr 4, s. 485-493
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URN: urn:nbn:se:ltu:diva-16023DOI: 10.1007/s10904-009-9290-8ISI: 000272035600008Scopus ID: 2-s2.0-77349115477Lokal ID: f9ae3100-672f-11de-9f57-000ea68e967bOAI: oai:DiVA.org:ltu-16023DiVA, id: diva2:988999
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Validerad; 2009; 20090702 (ysko)

Tilgjengelig fra: 2016-09-29 Laget: 2016-09-29 Sist oppdatert: 2023-10-14bibliografisk kontrollert

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