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Mesoporous Me-AlPO-5 spheres prepared using cation-exchange resins as templates
Luleå tekniska universitet.
Luleå tekniska universitet.
2004 (English)In: Recent advances in the science and technology of zeolites and related materials. Part A: proceedings of the International Zeolite Conference, Amsterdam: Elsevier, 2004, p. 660-666Conference paper, Published paper (Refereed)
Abstract [en]

Mesoporous self-bonded transition metal-containing AIPO-5 spheres were prepared by a multi-step procedure using macroporous cation exchange resin beads as a template. Aluminum was firstly introduced into the resin by ion exchange using an aluminum chlorohydrate solution. After separation and drying, tf Al-resin composite was mixed with phosphoric acid, tetraethylammonium hydroxide distilled water and hydrothermally treated to yield AIPO-5-resiii composite. Thereafter, vanadium or chromium were ion exchanged into the AIPO-5-resiii composites utilizing the residual ion exchange capacity of the resistor. Finally, the resin was combusted leaving behind Me-AlPO-5 (where Me is V or Cr) spheres similar in shaping and size to the original resin beads. The appearance of the spheres and the nature of the metal species were dependent on the metal loading. The metal introduction affected mainly the mesopore structure of the Mesophare AlPO-5 spheres.

Place, publisher, year, edition, pages
Amsterdam: Elsevier, 2004. p. 660-666
National Category
Chemical Process Engineering
Research subject
Chemical Technology
Identifiers
URN: urn:nbn:se:ltu:diva-28368Local ID: 225b14f0-9213-11db-8975-000ea68e967bISBN: 0-444-51827-4 (print)OAI: oai:DiVA.org:ltu-28368DiVA, id: diva2:1001564
Conference
International Zeolite Conference : 25/04/2004 - 30/04/2004
Note
Godkänd; 2004; 20060922 (bajo)Available from: 2016-09-30 Created: 2016-09-30 Last updated: 2017-11-25Bibliographically approved

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Sterte, Johan

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