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Solvent-free aminocarbonylation of iodobenzene in the presence of SILP-palladium catalysts
University of Pannonia, Institute of Chemistry, Department of Organic Chemistry, Hungary.
University of Pannonia, Institute of Chemistry, Department of Analytical Chemistry, Hungary.ORCID iD: 0000-0002-0271-4846
Hungarian Academy of Sciences, Centre for Energy Research, Department of Surface Chemistry and Catalysis, Hungary.
University of Pannonia, Institute of Chemistry, Department of Organic Chemistry, Hungary.
2016 (English)In: RSC Advances, ISSN 2046-2069, E-ISSN 2046-2069, Vol. 6, no 51, p. 45349-45356Article in journal (Refereed) Published
Abstract [en]

Heterogeneous palladium catalysts were prepared by the immobilisation of palladium on supported ionic liquid phases (SILP) obtained by physisorption or grafting. They were characterised by different techniques such as 13C CP MAS NMR, 31P CP MAS NMR, FT-IR, XPS and ICP. The catalysts were used efficiently under solvent-free conditions. They led to the formation of amide products with good to excellent selectivity. Recyclability at 5–10 bar CO pressure has also been demonstrated. The same reusable catalysts were proved to lead to the selective formation of double carbonylation products under higher pressure in DMF.

Place, publisher, year, edition, pages
Royal Society of Chemistry, 2016. Vol. 6, no 51, p. 45349-45356
National Category
Organic Chemistry Other Physics Topics
Research subject
Applied Physics
Identifiers
URN: urn:nbn:se:ltu:diva-66492DOI: 10.1039/C6RA03916BISI: 000376120100047Scopus ID: 2-s2.0-84969981095OAI: oai:DiVA.org:ltu-66492DiVA, id: diva2:1155552
Available from: 2017-11-08 Created: 2017-11-08 Last updated: 2017-11-29Bibliographically approved

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Szabó, Péter

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