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Laser surface hardening of 11% Cr ferritic stainless steel and its sensitisation behaviour
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Product and Production Development.ORCID iD: 0000-0002-9010-1555
Outokumpu Stainless Oy.
Outokumpu Stainless Oy.
Materials and Production Engineering, University of Oulu, Oulu, Finland.
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2018 (English)In: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 344, p. 673-679Article in journal (Refereed) Published
Abstract [en]

11% Cr ferritic stainless steel conforming to EN 1.4003 standard was surface hardened by a continuous-wave fibre laser beam. Both single-pass and multi-pass laser hardening was investigated. Different laser parameters were compared and their influence on hardness, microstructure, geometry of the hardened zone and sensitisation was investigated, especially for overlapping passes. The experiments showed that a surface hardness which is double that of the base material hardness was obtainable via martensitic phase transformation and high cooling rate, in spite of the low carbon and nitrogen content. This behaviour could be predicted from the chemical composition using the Kaltenhauser Ferrite Factor. Hardening at higher power levels gives more coarse-grained lath martensite but does not increase the hardness. Sensitisation was not a problem in single-pass hardening. However, the production of overlapping tracks could be detrimental to corrosion resistance in 11% Cr steel due to the formation of chromium carbides and nitrides.

Place, publisher, year, edition, pages
Elsevier, 2018. Vol. 344, p. 673-679
Keywords [en]
Laser surface hardening, Ferritic stainless steel, Sensitisation
National Category
Mechanical Engineering Manufacturing, Surface and Joining Technology
Research subject
Manufacturing Systems Engineering
Identifiers
URN: urn:nbn:se:ltu:diva-67581DOI: 10.1016/j.surfcoat.2018.04.002ISI: 000437391300077Scopus ID: 2-s2.0-85044924333OAI: oai:DiVA.org:ltu-67581DiVA, id: diva2:1181616
Note

Validerad;2018;Nivå 2;2018-04-06 (andbra)

Available from: 2018-02-09 Created: 2018-02-09 Last updated: 2022-06-30Bibliographically approved
In thesis
1. Aspects of Heat Flow in Laser Processing of Metals
Open this publication in new window or tab >>Aspects of Heat Flow in Laser Processing of Metals
2018 (English)Doctoral thesis, comprehensive summary (Other academic)
Abstract [en]

Since the laser was invented in 1960, its use in manufacturing industry has been growing rapidly. Laser processing of metals is based on the flow of heat that is generated by the absorbed laser beam. One outstanding aspect of laser beams is high precision along with high controllability of energy transfer, which includes creative techniques of shaping the beam and in turn the process. The thesis presents six Papers A-F on different metal processing techniques, namely welding, hardening and cutting, the latter combined with additive manufacturing. For each respective technique it was studied how desired properties can be optimized by controlled use of the laser beam and in turn of the temperature field. Addressing their different complexity of the heat transfer, various theoretical and experimental analysis methods were applied.

Laser beam welding is usually conducted with standard beam shapes, i.e. Gaussian or top-hat like, which is not always optimal for the process. Identification of an optimised weld pool shape or temperature cycle could increase the quality of welded products or even enable new applications. Papers A and B aim to increase the knowledge for non-standard beam shapes, particularly for single-pulse conduction mode welding. Paper A presents an investigation on an industrial application where a C-shaped weld joint is desired. The sensitivity to and optimization of different C-shaped beam irradiation profiles is discussed. The analysis is mainly carried out by applying Finite Element Analysis, FEA, to calculate the heat conduction contributions, showing unexpected sensitivity in certain regimes. Paper B presents a semi-analytical model for fast calculation of the temperature field from different beam profiles. Examples include multi-spots or the misalignment sensitivity of Diffractive Optical Elements.

In Paper C, for laser hardening of 11% Cr ferritic stainless steel the temperature field was studied to enable hardening. It was shown that single-track hardening without sensitisation could be achieved but overlapping tracks had a continuous network of ditched grain boundaries and is thereby at risk for sensitisation. The sensitised area is caused by a reheating cycle.

The same mechanism for the same material was studied in Paper D when applying a recently developed drop deposition technique, where additive manufacturing is fed by laser cutting. The same reheating isotherm becomes critical, but here sensitisation tests show a discontinuous network of ditched grain boundaries in the added material. The solid heat-affected zone on the other hand has a continuous network of ditched grain boundaries, which implies a sensitisation risk. The continuous network is however not in contact with the surface. The tested parameters is thus not at risk for intergranular corrosion through sensitisation.

For friction stir welding of dissimilar metals, Ti-6Al-4V with AISI 304L stainless steel, Paper E, the influence of a laser-induced preheating temperature field on the tool forces was investigated through numerical simulation. By suitable application of laser preheating, the forces acting on the tool can be substantially lowered, in a robust manner.

The temperature field from seam welding induces a residual stress field. In Paper F, for continuous wave laser keyhole welding of high strength steel butt joints, a method is presented to identify the residual stress behaviour of laser welded sheets by measurement of the fatigue crack growth rate during testing, by deriving the crack acceleration. The analysis was confirmed by hole drilling tests and by FEA.

The knowledge and methods of the above different experimental and theoretical studies complement each other. They contribute to further optimize certain aspects through laser-induced temperature fields, for different manufacturing techniques.

Place, publisher, year, edition, pages
Luleå: Luleå University of Technology, 2018
Series
Doctoral thesis / Luleå University of Technology 1 jan 1997 → …, ISSN 1402-1544
National Category
Mechanical Engineering Manufacturing, Surface and Joining Technology
Research subject
Manufacturing Systems Engineering
Identifiers
urn:nbn:se:ltu:diva-67586 (URN)978-91-7790-051-1 (ISBN)978-91-7790-052-8 (ISBN)
Public defence
2018-04-11, E632, Luleå, 09:00 (English)
Opponent
Supervisors
Available from: 2018-02-13 Created: 2018-02-09 Last updated: 2018-03-20Bibliographically approved

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Sundqvist, JesperKaplan, Alexander F. H.

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