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Self-Assembly and Exfoliation of a Molecular Solid Based on Cooperative B-N and Hydrogen Bonds
Dipartimento di Chimica “Giacomo Ciamician”, Università; di Bologna, Bologna, Italy.
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Material Science. CNR-IMM, Area della Ricerca di Bologna, Bologna, Italy.ORCID iD: 0000-0003-4598-9556
Dipartimento di Chimica “Giacomo Ciamician”, Università; di Bologna, Bologna, Italy.
Dipartimento di Chimica “Giacomo Ciamician”, Università; di Bologna, Bologna, Italy.
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2018 (English)In: Crystal Growth & Design, ISSN 1528-7483, E-ISSN 1528-7505, Vol. 18, no 12, p. 7259-7263Article in journal (Refereed) Published
Abstract [en]

Herein we report that 4-pyridinylboronic acid (1) in the solid state self-assembles into tetrameric macrocycles via B-N bond formation. The tetramers are linked via O-H···O bonds resulting in a material that can be exfoliated via sonication to give thinner sheets as we demonstrate via Fourier transform infrared spectroscopy, transmission electron microscopy, selected area electron diffraction, and atomic force microscopy experiments. For comparison, the structure of the related compound 4-(pyridin-4-yl) phenylboronic acid (2) is also discussed

Place, publisher, year, edition, pages
American Chemical Society (ACS), 2018. Vol. 18, no 12, p. 7259-7263
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Experimental Physics
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URN: urn:nbn:se:ltu:diva-72522DOI: 10.1021/acs.cgd.8b01674ISI: 000452694000005Scopus ID: 2-s2.0-85058136561OAI: oai:DiVA.org:ltu-72522DiVA, id: diva2:1278283
Available from: 2019-01-14 Created: 2019-01-14 Last updated: 2019-02-01Bibliographically approved

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Mazzaro, Raffaello

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