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Measuring the fracture toughness of single WC grains of cemented carbides by means of microcantilever bending and micropillar splitting
CIEFMA - Department of Materials Science and Engineering, EEBE, Universitat Politècnica de Catalunya-BarcelonaTECH, Avda. Eduard Maristany 16, 08019 Barcelona, Spain.
Eurecat, Centre Tecnològic de Catalunya, Unit of Metallic and Ceramic Materials, Plaça de la Ciència, 2, Manresa 08243, Spain.
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Mechanics of Solid Materials. Eurecat, Centre Tecnològic de Catalunya, Unit of Metallic and Ceramic Materials, Plaça de la Ciència, 2, Manresa 08243, Spain.ORCID iD: 0000-0003-4720-7888
CIEFMA - Department of Materials Science and Engineering, EEBE, Universitat Politècnica de Catalunya-BarcelonaTECH, Avda. Eduard Maristany 16, 08019 Barcelona, Spain. Barcelona Research Center in Multiscale Science and Engineering- Universitat Politècnica de Catalunya-BarcelonaTECH, Avda. Eduard Maristany 16, 08019 Barcelona, Spain.
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2021 (English)In: International journal of refractory metals & hard materials, ISSN 0263-4368, Vol. 98, article id 105529Article in journal (Refereed) Published
Abstract [en]

The main goal of this work is to obtain a reliable value of the fracture toughness of single grains of tungsten carbide (WC). It is attempted by testing microcantilever and micropillar samples shaped out, by means of focused ion beam milling, of individual WC particles embedded within a WC-Co cemented carbide grade. Experimental testing included the use of a nanoindenter for inducing microcantilever bending and micropillar splitting, as well as sampling WC grains with basal and prismatic orientations. Experimental results are compared with those previously assessed through implementation of the indentation microfracture technique. Bending of notched microcantilevers yielded more consistent results than those measured out of micropillar splitting tests. In this regard, the average value of fracture toughness for single WC grains, within the two-phase interpenetrated network existing in cemented carbides, is found to be 5.6 ± 0.8 MPa·m1/2. Such a relatively high value – coherent with local plastic features evidenced in nanoindentation imprints - is in satisfactory agreement with results indirectly estimated from other macromechanical tests.

Place, publisher, year, edition, pages
Elsevier, 2021. Vol. 98, article id 105529
Keywords [en]
Fracture toughness, WC grains, Mechanical properties, Micromechanical testing
National Category
Metallurgy and Metallic Materials
Research subject
Solid Mechanics
Identifiers
URN: urn:nbn:se:ltu:diva-83403DOI: 10.1016/j.ijrmhm.2021.105529ISI: 000663404900005Scopus ID: 2-s2.0-85103324731OAI: oai:DiVA.org:ltu-83403DiVA, id: diva2:1539831
Note

Validerad;2021;Nivå 2;2021-04-13 (johcin);

Finansiär: Spanish Ministry of Science, Innovation and Universities (PGC2018-096855-B-C41)

Available from: 2021-03-25 Created: 2021-03-25 Last updated: 2022-09-15Bibliographically approved

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