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Synthesis and synthetic applications of (4-hydroxyphenyl)perfluoroalkylmethanols
Division of Applied Chemistry, Institute of Engineering, Tokyo University of Agriculture and Technology, 2-24-16 Nakamachi, Koganei, 184-8588, Japan.
Division of Applied Chemistry, Institute of Engineering, Tokyo University of Agriculture and Technology, 2-24-16 Nakamachi, Koganei, 184-8588, Japan.
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Machine Elements.ORCID iD: 0000-0002-8972-2944
Division of Applied Chemistry, Institute of Engineering, Tokyo University of Agriculture and Technology, 2-24-16 Nakamachi, Koganei, 184-8588, Japan.ORCID iD: 0000-0002-1460-3086
2022 (English)In: Tetrahedron, ISSN 0040-4020, E-ISSN 1464-5416, Vol. 104, article id 132574Article in journal (Refereed) Published
Abstract [en]

Development of the convenient method for the synthesis of (hydroxyphenyl)perfluoro-alkylmethanols was achieved by the Meerwein-Ponndorf-Verley (MPV) type reduction of the in situ-generated perfluoroalkylated ketones as the key step. The benzylic OH group of the resultant alcohols was successfully converted to H or Rf(CH2)nO by way of the corresponding chlorides, this transformation being not easy by any other methods.
Place, publisher, year, edition, pages
Elsevier, 2022. Vol. 104, article id 132574
Keywords [en]
Perfluoroalkyl, Reduction, p-quinone methide, POSS
National Category
Organic Chemistry
Research subject
Machine Elements
Identifiers
URN: urn:nbn:se:ltu:diva-88027DOI: 10.1016/j.tet.2021.132574ISI: 000853078400006Scopus ID: 2-s2.0-85120311031OAI: oai:DiVA.org:ltu-88027DiVA, id: diva2:1614570
Note

Validerad;2022;Nivå 2;2022-03-04 (hanlid)

Available from: 2021-11-26 Created: 2021-11-26 Last updated: 2022-09-23Bibliographically approved

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Minami, Ichiro

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