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Characterization of Spark Plasma Sintered Graphene-Coated Stainless-Steel Compacts
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Material Science.ORCID iD: 0000-0003-2943-3654
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Material Science.ORCID iD: 0000-0003-4888-6237
Graphmatech AB, 753 18 Uppsala, Sweden.
2022 (English)Conference paper, Oral presentation only (Other academic)
Abstract [en]

We investigated the effect of sintering temperature and graphene content on the microstructure, densification, hardness, and wear properties of spark-plasma sintered (SPS) graphene-coated 316L stainless-steel powders. Four sintering temperatures (850, 900, 950, and 1000 °C) and graphene content of 0.01, 0.1, and 0.5 wt.% were investigated. Results showed that sintered density increased with the sintering temperature. Microstructural examination corroborated this result as distinct unsintered powder particles, sinter necks and large interparticle pores observed at 850 °C were annihilated at 1000 °C. The 316L stainless steel sintered specimen had a density of 7.27 g/cm3, which decreased slightly with increasing graphene content to 7.17 g/cm3 for the sample with 0.5 wt.% graphene coating. The sintering temperature and graphene content appeared not to have significant effect on the microhardness. For instance, microhardness for the reference 316L sintered specimen was 189 HV, compared to ~ 171 HV for all the graphene-coated 316L sintered specimens. X-ray diffraction analysis did not detect the formation of carbides in the sintered samples, which suggested that the sintering process minimized its formation. Raman spectroscopy indicated that sintering at 850 °C preserved the structure of graphene during the spark plasma sintering process. 

Place, publisher, year, edition, pages
2022.
National Category
Metallurgy and Metallic Materials
Research subject
Engineering Materials
Identifiers
URN: urn:nbn:se:ltu:diva-92393OAI: oai:DiVA.org:ltu-92393DiVA, id: diva2:1686084
Conference
11th EEIGM International Conference on Advanced Materials Research, Barcelona, Spain, June 16-17, 2022
Funder
Swedish Foundation for Strategic Research, RIF014-0083Available from: 2022-08-08 Created: 2022-08-08 Last updated: 2024-01-08Bibliographically approved

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Akinwekomi, Akeem DamilolaAkhtar, Farid

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