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Tetraphenyl- and tetratolylantimony complexes with N,N-dialkyldithiocarbamate ligands: synthesis, X-ray diffraction analysis, and 13C and 15N CP/MAS NMR studies
Blagoveshchensk State Pedagogical University.
Russian Adademy of Sciences.
Russian Adademy of Sciences.
Luleå University of Technology, Department of Civil, Environmental and Natural Resources Engineering, Sustainable Process Engineering.
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2006 (English)In: Russian journal of coordination chemistry, ISSN 1070-3284, E-ISSN 1608-3318, Vol. 32, no 6, p. 403-412Article in journal (Refereed) Published
Abstract [en]

Crystalline tetraphenylantimony and tetratolylantimony complexes with N,N-dialkyldithiocarbamate ligands [Sb(C6H5)4(S2CNR2)] (R = CH3, C2H5, and C3H7 and R2 = (CH2)6) were synthesized by ligand exchange reactions and studied by 13C and 15N CP/MAS NMR spectroscopy. X-ray diffraction analysis revealed that the complex [Sb(n-CH3-C6H4)4{S2CN(C3H7)2}] exists as the single molecular form, while [Sb(C6H5)4{S2CN(CH2)6}] exists as two molecular conformers. The 13C and 15N signals were assigned to the positions of the atoms in the isomeric structures [Sb(C6H5)4{S2CN(CH2)6}] in terms of different degrees of double bonding in the formally single =N-C(S)S-bond.

Place, publisher, year, edition, pages
2006. Vol. 32, no 6, p. 403-412
National Category
Physical Chemistry
Research subject
Chemistry of Interfaces
Identifiers
URN: urn:nbn:se:ltu:diva-3308DOI: 10.1134/S1070328406060017Local ID: 11d4ed20-d789-11db-a1bf-000ea68e967bOAI: oai:DiVA.org:ltu-3308DiVA: diva2:976165
Note
Validerad; 2006; 20070216 (bajo)Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2017-11-24Bibliographically approved

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