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Monitoring of antisolvent addition crystallization with Raman spectroscopy
Michigan State University.
Luleå University of Technology, Department of Civil, Environmental and Natural Resources Engineering, Sustainable Process Engineering.
2003 (English)In: Crystal Growth & Design, ISSN 1528-7483, E-ISSN 1528-7505, Vol. 3, no 6, p. 947-952Article in journal (Refereed) Published
Abstract [en]

Fiber optic Raman spectroscopy was used for in situ monitoring of antisolvent addition crystallization of cortisone acetate. Raman spectral features of the solvent, the antisolvent, and the solute were monitored to measure the relative concentration of the components. Different rates of antisolvent addition were monitored and the resulting solid-state form was characterized using Raman spectroscopy and DSC. Raman spectroscopy was used to monitor dehydration during storage of the product crystals. The current study demonstrates the advantages of using Raman spectroscopy to monitor the solution phase during crystallization and simultaneously monitoring the solid-state form.

Place, publisher, year, edition, pages
2003. Vol. 3, no 6, p. 947-952
National Category
Bioprocess Technology
Research subject
Biochemical Process Engineering
Identifiers
URN: urn:nbn:se:ltu:diva-3993DOI: 10.1021/cg0340446ISI: 000186481600011Scopus ID: 2-s2.0-0345014900Local ID: 1d96e1e0-2021-11dd-8447-000ea68e967bOAI: oai:DiVA.org:ltu-3993DiVA, id: diva2:976855
Note
Validerad; 2003; 20080512 (bajo)Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2018-07-10Bibliographically approved

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Berglund, Kris

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