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Solid state 31P and 207Pb MAS NMR studies on polycrystalline O,O′-dialkyldithiophosphate lead(II) complexes
Luleå University of Technology, Department of Civil, Environmental and Natural Resources Engineering, Sustainable Process Engineering.
Luleå University of Technology, Department of Civil, Environmental and Natural Resources Engineering, Sustainable Process Engineering.
Materials and Engineering Science, ANSTO.
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2005 (English)In: Journal of magnetic resonance, ISSN 1090-7807, E-ISSN 1096-0856, Vol. 177, no 1, p. 56-66Article in journal (Refereed) Published
Abstract [en]

A number of lead(II) O,O′-dialkyldithiophosphate complexes were studied by 13C, 31P, and 207Pb MAS NMR. Simulations of 31P chemical shift anisotropy using spinning sideband analysis reveal a linear relationship between the SPS bond angle and the principal values δ22 and δ33 of the 31P chemical shift tensor. The 31P CSA data were used to assign ligands with different structural functions. In the cases of Adiethyldithiophosphate and di-iso-butyldithiophosphate lead(II) complexes, 2J (31P, 207Pb)-couplings were resolved and used to confirm the suggested assignment of the ligands. The SIMPSON computer program was used to calculate 31P and 207Pb spectral sideband patterns.

Place, publisher, year, edition, pages
2005. Vol. 177, no 1, p. 56-66
National Category
Physical Chemistry
Research subject
Chemistry of Interfaces
Identifiers
URN: urn:nbn:se:ltu:diva-4820DOI: 10.1016/j.jmr.2005.07.007Local ID: 2cfc2b90-c726-11db-98d9-000ea68e967bOAI: oai:DiVA.org:ltu-4820DiVA: diva2:977694
Note
Validerad; 2005; 20070228 (bajo)Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2017-11-24Bibliographically approved

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Larsson, Anna-CarinIvanov, Alexander V.Forsling, WillisAntzutkin, Oleg
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