Influence of sputtering target power on microstructure and mechanical properties of W-N and Ta-N coatingsShow others and affiliations
2012 (English)In: Nanoscience and Nanotechnology Letters, ISSN 1941-4900, E-ISSN 1941-4919, Vol. 4, no 6, p. 604-608Article in journal (Refereed) Published
Abstract [en]
W-N and Ta-N coatings were manufactured using r.f. reactive magnetron sputtering technique in mixed atmosphere of Ar+N 2. The effect of sputtering power on the microstructure and mechanical properties of these coatings has been investigated. It was found that increasing sputtering power induced structure transformation of W-N and Ta-N coatings from hexagonal WN to fcc ω-W2N and from fcc TaN through a mixture of orthorhombic Ta3N5 and fcc TaN to orthorhombic Ta3N5, respectively. The increase in sputtering power led to grain refinement which played a major role in hardness enhancement. At the highest sputtering power of 100W, the average grain size of Ta-N and W-N coatings reduced to minimum value of 7 nm and 21 nm, correspondingly the hardness reached maximum value of 29 GPa and 31 GPa, respectively. However, Ta-N and W-N coatings possessed the biggest adhesion strength of ̃41 N and ̃48 N at the lowest sputtering power of 40 W and 25 W, respectively.
Place, publisher, year, edition, pages
2012. Vol. 4, no 6, p. 604-608
National Category
Tribology (Interacting Surfaces including Friction, Lubrication and Wear)
Research subject
Machine Elements
Identifiers
URN: urn:nbn:se:ltu:diva-5738DOI: 10.1166/nnl.2012.1372ISI: 000307195900005Scopus ID: 2-s2.0-84864855322Local ID: 3eb461f9-5f12-43ab-acd7-4678e7e90738OAI: oai:DiVA.org:ltu-5738DiVA, id: diva2:978613
Note
Godkänd; 2012; 20120820 (andbra)
2016-09-292016-09-292018-07-10Bibliographically approved