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ESR and Solid-State Natural Abundance 13 C CP/MAS NMR Study of Crystalline Alkyl (R=C 2 H 5 , i- C 3 H 7 , i- C 4 H 9 , s- C 4 H 9 , C 5 H 11 ) Xanthate Copper(II) and Thallium(I) Complexes.
Luleå University of Technology, Department of Civil, Environmental and Natural Resources Engineering, Sustainable Process Engineering.
Blagoveshchensk State Pedagogical University.
Luleå University of Technology, Department of Civil, Environmental and Natural Resources Engineering, Sustainable Process Engineering.ORCID iD: 0000-0003-1067-7990
2005 (English)In: Russian journal of coordination chemistry, ISSN 1070-3284, E-ISSN 1608-3318, Vol. 31, no 1, p. 45-50Article in journal (Refereed) Published
Abstract [en]

Crystalline thallium(I) alkylxanthate complexes [Tl{S(S)COR}]n (R = C2H5, i-C3H7, i-C 4H9, s-C4H9, and C5H 11) and isotope-substituted heteropolynuclear Cu(II)Tl(I) complexes [63(65)CuTl6(S2COR)8] (R= i-C 4H9 and C5H11) were obtained and studied by ESR and high-resolution solid-state 13C CP/MAS NMR spectroscopy. According to the 13C NMR data, polynuclear thallium(I) complexes contain structurally equivalent alkylxanthate ligands. The ESR study revealed the Jahn-Teller dynamic effect in Cu(II)Tl(I) complexes; the nuclei of six Tl atoms are involved in the hyperfine interaction

Place, publisher, year, edition, pages
2005. Vol. 31, no 1, p. 45-50
National Category
Physical Chemistry
Research subject
Chemistry of Interfaces
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URN: urn:nbn:se:ltu:diva-6189DOI: 10.1007/s11173-005-0047-9ISI: 000226914200008Local ID: 462e1180-c8bd-11db-98d9-000ea68e967bOAI: oai:DiVA.org:ltu-6189DiVA, id: diva2:979066
Note
Validerad; 2005; 20061220 (bajo)Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2018-07-10Bibliographically approved

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Ivanov, Alexander V.Antzutkin, OlegForsling, Willis

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