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ATR FTIR spectroscopy for in situ measurement of supersaturation
Michigan State University.
1997 (English)In: Journal of Crystal Growth, ISSN 0022-0248, E-ISSN 1873-5002, Vol. 179, no 1-2, p. 185-193Article in journal (Refereed) Published
Abstract [en]

The current contribution establishes the technical feasibility of Attenuated Total Reflection (ATR) Fourier transform infrared (FTIR) spectroscopy for the in situ measurement of supersaturation in crystallization processes. The approach was inspired by recent advancements in ATR spectroscopy by way of various light transfer systems for remote sensing and by the increasing availability of ATR configurations well suited for remote, in situ measurements. The feasibility of the technique was investigated using a DIPPER-210® immersion probe manufactured by Axiom Analytical, Inc. Initial experiments conducted using aqueous maleic acid proved that ATR FTIR spectroscopy can be successfully employed to measure supersaturation, solubility and the metastable limit, in situ, with sufficient accuracy and precision.

Place, publisher, year, edition, pages
1997. Vol. 179, no 1-2, p. 185-193
National Category
Bioprocess Technology
Research subject
Biochemical Process Engineering
Identifiers
URN: urn:nbn:se:ltu:diva-7022DOI: 10.1016/S0022-0248(97)00119-XLocal ID: 55a2e060-3bc4-11de-a8ec-000ea68e967bOAI: oai:DiVA.org:ltu-7022DiVA, id: diva2:979909
Note
Upprättat; 1997; 20090508 (ysko)Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2017-11-24Bibliographically approved

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Berglund, Kris

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