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Covalent Functionalization of HiPco Single-Walled Carbon Nanotubes: Differences in the Oxidizing Action of H2SO4 and HNO3 during a Soft Oxidation Process
Institut Jean Lamour, Department P2M, UMR 7198 CNRS–Université de Lorraine, Ecole des Mines, 54042 Nancy.
Institut Jean Lamour, CNRS – Nancy Université, Laboratoire de Chimie du Solide Minéral, Nancy Université.
Institut Jean Lamour, CNRS – Nancy Université, Laboratoire de Chimie du Solide Minéral, Nancy Université.
Institut Jean Lamour, Nancy Universite.
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2015 (English)In: ChemPhysChem, ISSN 1439-4235, E-ISSN 1439-7641, Vol. 16, no 12, p. 2692-2701Article in journal (Refereed) Published
Abstract [en]

The results of a study on the evolution of HiPco single-walled carbon nanotubes during the oxidizing action of H2SO4 and HNO3 are presented. The process conditions used have been chosen so as to avoid any significant damage to the nanotube structure. The type and level of functionalization, the location of the grafted functions on the surface of the nanotube and the changes in morphological characteristics of the samples were examined by using a wide and complementary range of analytical techniques. We propose an explanation for the differences in the oxidizing action of sulfuric and nitric acids. The combined results allow us to suggest possible reaction mechanisms that occur on the surface of the nanotube.

Place, publisher, year, edition, pages
2015. Vol. 16, no 12, p. 2692-2701
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Experimental physics
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URN: urn:nbn:se:ltu:diva-7362DOI: 10.1002/cphc.201500248ISI: 000359906900026PubMedID: 26136373Scopus ID: 2-s2.0-84939252266Local ID: 5bc47731-9547-4a86-99ba-8d3283d0a889OAI: oai:DiVA.org:ltu-7362DiVA, id: diva2:980251
Note
Validerad; 2015; Nivå 2; 20150703 (andbra)Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2018-07-10Bibliographically approved

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Allali, NaoualSoldatov, Alexander

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