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Alternative method to precipitation techniques for synthesizing yttrium oxide nanopowder
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Material Science.ORCID iD: 0000-0002-2286-5588
2007 (English)In: Powder Technology, ISSN 0032-5910, E-ISSN 1873-328X, Vol. 177, no 2, p. 77-82Article in journal (Refereed) Published
Abstract [en]

Yttrium oxide nano-powder has been successfully synthesized by a novel approach. In the first step, a foamy structure was produced by combustion synthesis using yttrium nitrate and glycine. This was followed by the addition of sulfate ions and calcination at 1100 °C for 4 h. The sulfated and unsulfated powders were characterized by X-ray powder diffraction (XRD), scanning electron microscope (SEM), transmission electron microscopy (TEM) and the Brunauer-Emmett-Teller method (BET). The sinterability of the resulting powders was also studied by dilatometry. The studies indicated that this method not only allows for producing weakly-agglomerated nano-particles, but is also a very time-efficient process in comparison to precipitation techniques. Moreover, the possibility of performing all processing steps in a fully automated batch reactor was also considered.

Place, publisher, year, edition, pages
2007. Vol. 177, no 2, p. 77-82
National Category
Other Materials Engineering
Research subject
Engineering Materials
Identifiers
URN: urn:nbn:se:ltu:diva-7376DOI: 10.1016/j.powtec.2007.02.045Local ID: 5bf6c620-773a-11dc-80da-000ea68e967bOAI: oai:DiVA.org:ltu-7376DiVA: diva2:980265
Note
Validerad; 2007; 20071010 (bajo)Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2017-11-24Bibliographically approved

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