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Determination of 60 elements in whole blood by sector field inductively coupled plasma mass spectrometry
Luleå University of Technology, Department of Civil, Environmental and Natural Resources Engineering, Geosciences and Environmental Engineering.ORCID iD: 0000-0003-4505-4590
Luleå tekniska universitet.
Luleå tekniska universitet.
2000 (English)In: Journal of Analytical Atomic Spectrometry, ISSN 0267-9477, E-ISSN 1364-5544, Vol. 15, no 8, p. 937-944Article in journal (Refereed) Published
Abstract [en]

A method is described for the determination of 60 elements in whole blood, using a double-focusing ICP-MS instrument. Microwave-assisted digestion in low-volume PFA vessels resulted in 10-fold sample dilution. External calibration with matrix-matched standards was used for quantification. Different factors affecting detection limits are discussed. The performance of the method for the determination of environmentally relevant concentrations was evaluated using a whole blood reference material and intercomparison samples. Owing to high instrumental detection power and low preparation blanks, 57 elements could be detected in the bovine whole blood reference material (IAEA A-13). Trace element leaching from commercially available blood sampling tubes made of glass was shown to be a serious contamination factor. Concentrations obtained for three calf blood samples taken under `metal-free' conditions are presented.

Place, publisher, year, edition, pages
2000. Vol. 15, no 8, p. 937-944
National Category
Geochemistry
Research subject
Applied Geology
Identifiers
URN: urn:nbn:se:ltu:diva-7567DOI: 10.1039/b003561kISI: 000088467600006Scopus ID: 2-s2.0-0034246126Local ID: 5f37a350-b79a-11db-abff-000ea68e967bOAI: oai:DiVA.org:ltu-7567DiVA, id: diva2:980457
Note
Validerad; 2000; 20070208 (ysko)Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2018-07-10Bibliographically approved

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Rodushkin, Ilya

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