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Tetraphenylantimony(V) O,O″-dialkyl dithiophosphates [Sb(C 6H5)4{S2P(OR)2}] (R = s-C4H9, c-C6H11): synthesis, structures, and 13C and 31P CP/MAS NMR spectra
Institute of Geology and Nature Management, Far East Branch, Russian Academy of Sciences, Blagoveshchensk.
Blagoveshchensk State Pedagogical University.
Luleå University of Technology, Department of Civil, Environmental and Natural Resources Engineering, Sustainable Process Engineering.
Institute of Chemistry, Far Eastern Branch of the Russian Academy of Sciences, 690022, Vladivostok.
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2008 (English)In: Russian journal of coordination chemistry, ISSN 1070-3284, E-ISSN 1608-3318, Vol. 34, no 7, p. 527-535Article in journal (Refereed) Published
Abstract [en]

Tetraphenylantimony(V) O,O′-di-sec-butyl dithiophosphate (I) and tetraphenylantimony(V) O,O′-dicyclohexyl dithiophosphate (II) [Sb(C 6H5)4{S2P(OR)2}] (R = sec-C4H9 or cyclo-C6H11) were obtained. Their structures and spectroscopic properties were studied by X-ray diffraction analysis and 13C and 31P CP/MAS NMR spectroscopy. The dithiophosphate (Dtph) ligands in complexes I and II were found to be coordinated in S-monodentate and S,S′-bidentate fashions, respectively (MAS NMR data). According to X-ray diffraction data, the coordination polyhedron of antimony in molecular structure I is a trigonal bipyramid with unusual monodentate coordination of the Dtph group in the axial position.

Place, publisher, year, edition, pages
2008. Vol. 34, no 7, p. 527-535
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Physical Chemistry
Research subject
Chemistry of Interfaces
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URN: urn:nbn:se:ltu:diva-8692DOI: 10.1134/S1070328408070099ISI: 000257592400009Scopus ID: 2-s2.0-47249084842Local ID: 73a817b0-7365-11dd-a60f-000ea68e967bOAI: oai:DiVA.org:ltu-8692DiVA, id: diva2:981630
Note
Validerad; 2008; 20080826 (ysko)Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2018-07-10Bibliographically approved

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Ivanov, Alexander V.Antzutkin, Oleg

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