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2-dimensional side-band separation in magic-angle-spinning NMR
Stockholm University.
Stockholm University.
1995 (English)In: Journal of Magnetic Resonance - Series A, ISSN 1064-1858, E-ISSN 1096-0864, Vol. 115, no 1, p. 7-19Article in journal (Refereed) Published
Abstract [en]

A new method for separating isotropic and anisotropic chemical-shift interactions in magic-angle-spinning NMR is presented. The new method is based upon manipulation of the phases of spinning sidebands using sequences of five π pulses. A two-dimensional pulse scheme separates the spinning sidebands by order. The amplitudes of the spinning sidebands may be analyzed to obtain the principal values of the chemical-shift anisotropy. For sites with many sidebands, it is possible to improve the signal-to-noise ratio considerably by skew projection of the two-dimensional spectrum. Experimental demonstrations are presented.

Place, publisher, year, edition, pages
1995. Vol. 115, no 1, p. 7-19
National Category
Physical Chemistry
Research subject
Chemistry of Interfaces
Identifiers
URN: urn:nbn:se:ltu:diva-9103DOI: 10.1006/jmra.1995.1142Local ID: 7ab04590-ec21-11db-88eb-000ea68e967bOAI: oai:DiVA.org:ltu-9103DiVA, id: diva2:982041
Note

Upprättat; 1995; 20070416 (bajo)

Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2017-11-24Bibliographically approved

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Antzutkin, Oleg

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