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Synthesis of thin silicalite-1 films on steel supports using a seeding method
Luleå tekniska universitet.
Luleå University of Technology, Department of Civil, Environmental and Natural Resources Engineering, Sustainable Process Engineering.
2002 (English)In: Microporous and Mesoporous Materials, ISSN 1387-1811, E-ISSN 1873-3093, Vol. 52, no 3, p. 191-197Article in journal (Refereed) Published
Abstract [en]

Thin and continuous silicalite-1 films with controllable thickness between 200 and 800 nm were synthesized on steel supports by a method employing seeding. A variety of steel types ranging from ordinary carbon steel to highly corrosion resistant steel were used. Continuous transparent silicalite-1 films were formed on all steel types after zeolite synthesis. The type of steel did not affect the film morphology, the thickness or the preferred orientation of the crystals. The (5 0 1) reflection dominates in the XRD pattern for thin films whereas the (1 0 1) and (3 0 3) reflections dominate for thicker films. The silicalite-1 films on various stainless steel supports were stable during calcination, whereas a relatively thick magnetite/hematite film formed on carbon steel upon calcination and the silicalite-1 film detached.

Place, publisher, year, edition, pages
2002. Vol. 52, no 3, p. 191-197
National Category
Chemical Process Engineering
Research subject
Chemical Technology
Identifiers
URN: urn:nbn:se:ltu:diva-9380DOI: 10.1016/S1387-1811(02)00319-0ISI: 000176019600006Scopus ID: 2-s2.0-0036576652Local ID: 7fd8dfc0-6f83-11db-962b-000ea68e967bOAI: oai:DiVA.org:ltu-9380DiVA, id: diva2:982318
Note
Validerad; 2002; 20060929 (bajo)Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2018-07-10Bibliographically approved

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Hedlund, JonasSterte, Johan

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