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Performance characteristics of a tandem spray chamber arrangement in double focusing sector field ICP-MS
Luleå tekniska universitet.
Luleå University of Technology, Department of Civil, Environmental and Natural Resources Engineering, Geosciences and Environmental Engineering.ORCID iD: 0000-0003-4505-4590
Luleå tekniska universitet.
2000 (English)In: Journal of Analytical Atomic Spectrometry, ISSN 0267-9477, E-ISSN 1364-5544, Vol. 15, no 6, p. 727-729Article in journal (Refereed) Published
Abstract [en]

A tandem cyclone-Scott type spray chamber configuration combined with infrared heating and a low-flow Micromist nebulizer was evaluated for the use in a ICP-SFMS sample introduction system. The system provides about a 3-fold sensitivity gain and lower oxide formation compared to the standard introduction system, although matrix-induced signal suppression is more pronounced, especially for elements with high ionization potential. The technique was evaluated by accurate analysis of riverine water reference material SLRS-3 with generally good agreement with certified and literature values. Long-term precision at a 20rµgrlm1 concentration level was 0.7% RSD in low resolution and 1.6% RSD in medium resolution. Precision in the range 0.03-0.09% RSD for lead isotope ratios at 1rµgrlm1 was obtained.

Place, publisher, year, edition, pages
2000. Vol. 15, no 6, p. 727-729
National Category
Geochemistry
Research subject
Applied Geology
Identifiers
URN: urn:nbn:se:ltu:diva-10949DOI: 10.1039/b002609nISI: 000087419300023Scopus ID: 2-s2.0-0033706823Local ID: 9d794d60-b779-11db-abff-000ea68e967bOAI: oai:DiVA.org:ltu-10949DiVA, id: diva2:983897
Note
Validerad; 2000; 20070208 (ysko)Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2018-07-10Bibliographically approved

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Rodushkin, Ilya

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