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Effect of temperature and atmosphere on fretting wear of self-mated Fe-10Cr-4Al alloy for nuclear power application
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Machine Elements.ORCID iD: 0000-0002-5593-1908
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Machine Elements.ORCID iD: 0000-0003-3123-0303
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Machine Elements.ORCID iD: 0000-0003-1454-1118
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Machine Elements.ORCID iD: 0000-0003-1162-4671
2025 (English)In: Wear, ISSN 0043-1648, E-ISSN 1873-2577, Vol. 564-565, article id 205704Article in journal (Refereed) Published
Abstract [en]

Over the years, fretting has been a leading cause of fuel failures for water cooled nuclear reactors. Implementation of liquid lead coolant increases the need for fretting and corrosion-resistant materials. Fe–10Cr–4Al alloy has shown good resistance to thermal aging, oxidation, liquid metal corrosion, and embrittlement in liquid lead environment. The performance of Fe-10Cr-4Al under fretting wear conditions has not been studied previously. This work aims to investigate the fretting wear and friction behaviour of self-mated Fe-10Cr-4Al alloy at varying temperatures, in the presence of a reducing gas environment and liquid lead. The results show that an increase in test temperature from RT to 550 °C decreases the coefficient of friction and promotes the formation of Cr and Fe oxide third body layer. At high temperature in reducing gas atmosphere, the initial plastic deformation and severe adhesion leads to early seizure. Presence of liquid lead has a lubricating effect and allows a third body layer to form on worn surfaces. A detailed description of the initial wear mechanisms of Fe-10Cr-4Al alloy and friction levels under various conditions provides a base for further investigation of this alloy for long-duration fretting wear.

 

Place, publisher, year, edition, pages
Elsevier, 2025. Vol. 564-565, article id 205704
Keywords [en]
Wear, Friction, High temperature fretting, Liquid lead
National Category
Other Mechanical Engineering Metallurgy and Metallic Materials
Research subject
Machine Elements
Identifiers
URN: urn:nbn:se:ltu:diva-111161DOI: 10.1016/j.wear.2024.205704ISI: 001391346100001Scopus ID: 2-s2.0-85212156825OAI: oai:DiVA.org:ltu-111161DiVA, id: diva2:1925420
Funder
Swedish Foundation for Strategic Research, ARC19-0043
Note

Validerad;2025;Nivå 2;2025-01-08 (signyg);

Fulltext license: CC BY

Available from: 2025-01-08 Created: 2025-01-08 Last updated: 2026-01-30Bibliographically approved
In thesis
1. On high temperature fretting in liquid lead
Open this publication in new window or tab >>On high temperature fretting in liquid lead
2026 (English)Doctoral thesis, comprehensive summary (Other academic)
Abstract [en]

The increasing interest in liquid metal cooled nuclear reactors provides technical and scientific challenges, such as the understanding, prevention, and prediction of the degradation of materials in liquid lead. This work examines fretting wear, occurring between the spacer wire wrapped around fuel tubes and between the steam generator tubes and their supports.

Studies of fretting in liquid lead often focus on the corrosive effects of lead and employ varying test methods. Comparing results from specially built equipment and widely used lab-scale test rigs is challenging because the rigs operate over different load ranges and in different environmental conditions. Publications on the topic lack detailed descriptions of wear mechanisms and friction data. At the same time, both short- and long-duration experiments under conditions relevant to nuclear reactor operation are necessary. This work aims to develop a simplified test methodology for new candidate materials intended for liquid-metal environments and to perform fretting tests on selected materials to understand the dominant wear mechanisms.

The modified oscillating friction and wear tester and the developed methodology were shown to be suitable for investigating fretting in liquid lead. The waviness of the test specimen surfaces significantly influences friction and wear behavior. Lower surface roughness showed superior fretting performance for self-mated Fe-10Cr-4Al, resulting in reduced local contact pressures that limit plastic deformation and material removal. The findings emphasize the importance of surface topography control in mitigating fretting damage in components.

The tribopair with one surface laser-clad with Fe-10Cr-4Al exhibited the lowest wear rate among all tested Fe-10Cr-4Al tribopairs. This is attributed to the difference in hardness between the specimens, which promotes distributed plastic deformation and the formation of a more uniform debris layer.

Fretting tests of self-mated Fe-10Cr-4Al alloy were performed using the modified friction and wear tester and a specially built equipment. After tests with an increasing number of cycles, similar wear mechanisms and wear depths were observed at both facilities. A reduced lubricating effect from saturated lead and its limited availability at the contact were shown to be the main damage-accelerating factors.

Place, publisher, year, edition, pages
Luleå tekniska universitet, 2026
Series
Doctoral thesis / Luleå University of Technology, ISSN 1402-1544
Keywords
fretting, liquid lead, friction, wear, high temperature
National Category
Other Mechanical Engineering
Research subject
Machine Elements
Identifiers
urn:nbn:se:ltu:diva-116252 (URN)978-91-8048-983-6 (ISBN)978-91-8048-984-3 (ISBN)
Public defence
2026-03-27, E231, Luleå University of Technology, Luleå, 09:00 (English)
Opponent
Supervisors
Available from: 2026-02-02 Created: 2026-01-30 Last updated: 2026-03-06Bibliographically approved

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Kolbas, D.Pelcastre, L.Prakash, B.Hardell, J.

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