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Textural and chemical characterization of sulfide minerals for improved beneficiation and exploration, Skellefte district, Sweden
Luleå University of Technology, Department of Civil, Environmental and Natural Resources Engineering, Geosciences and Environmental Engineering.ORCID iD: 0000-0001-8751-4116
2025 (English)Doctoral thesis, comprehensive summary (Other academic)
Abstract [en]

Volcanogenic massive sulfide (VMS) deposits belong to the most significant sources of base and precious metals such as Zn, Cu, Pb, Ag, and Au, as well as critical elements such as In, Ga, Ge, Sb, and Bi. Deformation and metamorphism of VMS deposits complicate their exploration and beneficiation. Examples are found in the Skellefte district, northern Sweden, where VMS deposits formed and underwent polyphase deformation (D1, D2, D3) during the 2.0–1.8 Ga Svecokarelian orogeny, imparting structural and mineralogical complexity at various scales. Presence of highly conductive graphitic strata in the host succession complicates direct detection using conventional electromagnetic geophysical techniques, necessitating a larger emphasis on geological and geochemical criteria to guide exploration. This study addresses these challenges by providing an integrated mineralogical, chemical, and textural characterisation of the Rävliden North Zn–Cu–Pb–Ag VMS deposit in the Skellefte district. 

Rävliden North is hosted at the transition between 1.89–1.88 Ga metavolcanic rocks of the Skellefte group and overlying 1.88–1.87 Ga, predominately metasedimentary rocks of the Vargfors group. Massive to semi-massive sphalerite, pyrrhotite, galena, pyrite occurs structurally and stratigraphically above chalcopyrite, pyrrhotite, pyrite-dominated mineralisation. Petrographic and structural analysis reveals textural evidence of sulfides hosted in ductile to brittle structures (e.g. foliations, boudinage, durchbewegt ore, piercement veins, tension gashes, breccia, and veinlets), indicative of polyphase remobilisation. Microanalysis show that sphalerite and chalcopyrite retain a zonation comparable with unmetamorphosed VMS, with enrichment of Cu, Co, and In in chalcopyrite-rich mineralisation. Limited syn-metamorphic redistribution of trace elements occurred beyond partitioning between coexisting sulfides. In-situ δ34S analyses indicate limited isotopic fractionation, with δ³⁴S values tightly constrained at 0 ± 2‰, consistent with a volcanic sulfur source. Meanwhile, variable δ114Cd, δ66Zn, δ56Fe and Zn/Cd ratios in sphalerite suggest an importance of mass-dependent kinetic fractionation with lighter isotopes precipitating near a high-temperature source, albeit volcanic source rocks akin to the Skellefte group can be pinpointed based on Pb isotopes. 

Overprinting, late-Svecokarelian sulfide assemblages (sphalerite, galena, Ag-rich sulfosalts) occur in quartz veins and sulfide-cemented breccia that crosscut ductile fabrics in the hanging wall. These host sphalerite and galena enriched in Cd, Ag, and Sb, and exhibit δ34S values consistent with recycling of syn-sedimentary sulfides, originally formed via sulfate reduction under anoxic deep-ocean conditions. Post-Svecokarelian mineralisation associated with calcite or zeolite (laumontite, heulandite and wairakite) veins and breccia crosscut all ductile fabrics. Distinctive colour-zoned sphalerite with oscillatory trace-element distribution in twins (enriched in Ga, Ge, Cu, Sb) together with δ114Cd, δ66Zn, δ56Fe, Zn/Cd, δ34S, δ15C and δ18O indicate a low-temperature (~150 °C) system involving reduced meteoric to connate water. Mineralogical and Pb isotopic similarities to nearby vein- and breccia-type Zn-Pb deposits indicate derivation from a juxtaposed mineral system at c. 0.5 Ga, linked to far field effects during opening of the Iapetus Ocean or the Timanian orogeny. Future research should test exploration vectors derived from hanging wall mineralisation, perhaps by correlating bulk-rock geochemical proxies with mineral-scale chemistry.

The classification of Rävliden North’s VMS mineralisation based on dominant sulfides, host lithology, and textures allowed the investigation of mineral processing performance. Massive sphalerite-rich mineralisation hosted in amphibole and mica rich rocks differ markedly in grindability and flotation response compared to chalcopyrite-rich veinlets in more quartz-rich rocks. Recovery and concentrate quality for Zn, Cu, and Pb are controlled by mineralogy, liberation and grain size, while trace and critical elements (Ag, Sb, Bi, Cd, Hg, Tl, As) recovery depends on liberation and inter-locking associations with sulfides and sulfosalts. The results allow optimisation of blending protocols that could help enhance recoveries, mitigate deleterious elements, and facilitate exploitation of future by-products such as Bi and Sb. Future research should develop geometallurgical models that capture deposit-scale variability and strategies to recover critical metals as by-products.

Place, publisher, year, edition, pages
Luleå: Luleå University of Technology, 2025.
Series
Doctoral thesis / Luleå University of Technology 1 jan 1997 → …, ISSN 1402-1544
Keywords [en]
VMS, exploration, mineral processing, mineral chemistry, mineralogy, metamorphism, deformation, remobilisation
National Category
Geology Mineral and Mine Engineering
Research subject
Ore Geology
Identifiers
URN: urn:nbn:se:ltu:diva-114811ISBN: 978-91-8048-905-8 (print)ISBN: 978-91-8048-906-5 (electronic)OAI: oai:DiVA.org:ltu-114811DiVA, id: diva2:1999144
Public defence
2025-11-14, C305, Luleå University of Technology, Luleå, 09:00 (English)
Opponent
Supervisors
Available from: 2025-09-19 Created: 2025-09-18 Last updated: 2025-10-24Bibliographically approved
List of papers
1. Ore Remobilization History of the Metamorphosed Rävliden North Volcanogenic Massive Sulfide Deposit, Skellefte District, Sweden
Open this publication in new window or tab >>Ore Remobilization History of the Metamorphosed Rävliden North Volcanogenic Massive Sulfide Deposit, Skellefte District, Sweden
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2024 (English)In: Economic geology and the bulletin of the Society of Economic Geologists, ISSN 0361-0128, E-ISSN 1554-0774, Vol. 119, no 4, p. 907-934Article in journal (Refereed) Published
Abstract [en]

The Skellefte district in northern Sweden hosts many volcanogenic massive sulfide (VMS) deposits and is considered one of the most important European mining districts for Cu, Zn, Pb, Ag, and Au. The volcanic and sedimentary rocks that the VMS deposits are hosted in were deformed during the Svecokarelian orogeny, with three documented regional deformation phases. These events imparted a distinct attitude and geometry to the deposits, their host succession, and discordant zones of synvolcanic hydrothermal alteration. Few studies have investigated the detailed deformation effects on the sulfide minerals.

In this contribution, we document the structural characteristics and remobilization history of mineralization at the Rävliden North Zn-Pb-Cu-Ag deposit—one of the most important recent discoveries in the district consisting of 8.5 million tonnes (Mt) grading 1.01% Cu, 3.45% Zn, 0.53% Pb, 78.60 g/t Ag, and 0.23 g/t Au. At Rävliden, massive to semimassive sphalerite-rich mineralization with lesser pyrrhotite, galena, pyrite, and silver minerals occurs structurally above stringer-type mineralization dominated by chalcopyrite, pyrrhotite, and pyrite. These mineralization types exhibit evidence of deformation and remobilization such as (1) sulfide-alignment parallel to tectonic foliations; (2) rounded wall-rock tectonoclasts in a ductile deformed sulfide matrix (“ball ore” or durchbewegt ore); and (3) sulfides in tension gashes, strain shadows, piercement veins, and late, straight veinlets crosscutting tectonic fabrics. These features are attributed to polyphase deformation during the D1, D2, and D3 events at temperature ranging from 200° to 550°C. Remobilization of sulfides was mostly within the bounds of the main mineralization (i.e., 10–100 m), with few local external occurrences. A combination of solid-state and fluid-assisted remobilization processes are inferred.

Rare brittle veinlets and zeolite-cemented breccias with sphalerite, galena, and silver minerals occur in the stratigraphic hanging wall, where they crosscut all Svecokarelian structures. This mineralization type is highly reminiscent of Phanerozoic low-T vein- and breccia-hosted Pb-Zn deposits of the Lycksele-Storuman area west of Rävliden North, which have been linked to far-field effects associated with the opening of the Iapetus Ocean (0.7–0.5 Ga). We suggest that this Zn-Pb mineralizing event led to the formation of the late sulfide-zeolite veinlets and breccias at Rävliden North, and that elements such as Ag and Sb within this mineralization were locally remobilized from Rävliden.

Place, publisher, year, edition, pages
Society of Economic Geologists, 2024
National Category
Geology
Research subject
Ore Geology
Identifiers
urn:nbn:se:ltu:diva-107577 (URN)10.5382/econgeo.5083 (DOI)001250593500002 ()2-s2.0-85196307375 (Scopus ID)
Funder
The Geological Survey of Sweden (SGU), 36-2031/2018
Note

Validerad;2024;Nivå 2;2024-06-27 (joosat);

Full text license: CC BY;

Funder: Boliden;

Available from: 2024-06-18 Created: 2024-06-18 Last updated: 2025-10-21Bibliographically approved
2. Redistribution of minor and trace elements in ore minerals in metamorphosed VMS deposits, Rävliden North, Skellefte district, Sweden
Open this publication in new window or tab >>Redistribution of minor and trace elements in ore minerals in metamorphosed VMS deposits, Rävliden North, Skellefte district, Sweden
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2025 (English)In: Journal of Geochemical Exploration, ISSN 0375-6742, E-ISSN 1879-1689, Vol. 278, article id 107830Article in journal (Refereed) Published
Abstract [en]

The Rävliden North volcanogenic massive sulfide (VMS) deposit, in northern Sweden underwent polyphase deformation and greenschist to lower amphibolite facies metamorphism during the Svecokarelian orogeny. This caused remobilisation and recrystallisation of ore minerals, whose composition was analysed using laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) and electron probe microanalysis (EPMA). Sphalerite, chalcopyrite, and pyrrhotite chemistry mirrors zonation of undeformed VMS deposits. Chalcopyrite-rich mineralisation contains higher Cu, Co, In, and lower Mn concentrations than sphalerite-rich mineralisation. Besides galena, Ag occurs in sulfosalts, tellurides, antimonides, and amalgams, which possibly formed through exsolutions from α-galena in syn- to post-tectonic structures. LA-ICP-MS imaging shows Ag-rich minerals in early syngenetic pyrite, in contrast to syn-metamorphic pyrite, indicating remobilisation during deformation. Despite sampling effects accounted for through linear mixed effects (LME) modelling, the results indicate that syn-metamorphic recrystallisation and remobilisation did not lead to substantial compositional changes in ore minerals. Instead, these processes partitioned Ga between sphalerite and chalcopyrite and enriched Ag, Cd, and Sb in minerals associated with younger parageneses. Zeolite-bearing veins in the hanging wall host sphalerite with the highest Ga, Ge, Cu, and Sb contents and galena with the lowest Bi, Te, and Tl contents. An origin potentially linked to far-field effects of the opening of the Iapetus Ocean or waning Timanian orogeny is discussed based on similarities to other vein- and breccia-hosted Zn Pb deposits in Northern Sweden. This study provides the first multiple-mineral in-situ trace element dataset for a VMS deposit in the Skellefte district, enhances understanding of element redistribution during metamorphism, and identifies remobilised elements potentially vectoring mineralisation at depth. Moreover, this study enables tracing of penalty and by-product elements in downstream beneficiation processes.

Place, publisher, year, edition, pages
Elsevier, 2025
Keywords
sulfide chemistry, trace elements, sulfosalt chemistry, metamorphosed VMS, LA-ICP-MS, EPMA
National Category
Geology
Research subject
Ore Geology
Identifiers
urn:nbn:se:ltu:diva-113017 (URN)10.1016/j.gexplo.2025.107830 (DOI)2-s2.0-105008003634 (Scopus ID)
Funder
The Geological Survey of Sweden (SGU), 36-2031/2018
Note

Validerad;2025;Nivå 2;2025-06-27 (u5);

Full text license: CC BY 4.0;

Funder: Boliden; Sveriges Ingenjörers Miljöfond (LTU-437-2024);

Available from: 2025-06-09 Created: 2025-06-09 Last updated: 2025-10-21Bibliographically approved
3. Isotopic fingerprinting of remobilised and superimposed mineralisation in orogenic terrains: Rävliden North VMS Deposit, Skellefte District, Sweden
Open this publication in new window or tab >>Isotopic fingerprinting of remobilised and superimposed mineralisation in orogenic terrains: Rävliden North VMS Deposit, Skellefte District, Sweden
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(English)Manuscript (preprint) (Other academic)
Keywords
VMS, metamorphism, isotope geochemistry, remobilisation, SIMS
National Category
Geology Geochemistry
Research subject
Ore Geology; Applied Geochemistry
Identifiers
urn:nbn:se:ltu:diva-114637 (URN)
Funder
The Geological Survey of Sweden (SGU), 36-2031/2018Vinnova, 2019-05167Swedish Research Council Formas, 2019-05167Swedish Energy Agency, 2019-05167
Available from: 2025-09-18 Created: 2025-09-18 Last updated: 2025-10-21Bibliographically approved
4. The role of ore and host rock mineralogy in the beneficiation of a VMS deposit: insights from Rävliden North, northern Sweden
Open this publication in new window or tab >>The role of ore and host rock mineralogy in the beneficiation of a VMS deposit: insights from Rävliden North, northern Sweden
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(English)Manuscript (preprint) (Other academic)
National Category
Mineral and Mine Engineering Geology
Research subject
Ore Geology
Identifiers
urn:nbn:se:ltu:diva-114635 (URN)
Funder
The Geological Survey of Sweden (SGU), 36-2031/2018
Available from: 2025-09-18 Created: 2025-09-18 Last updated: 2025-10-21Bibliographically approved

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