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ZSM-5 structured catalysts coated with silicalite-1
Luleå University of Technology, Department of Civil, Environmental and Natural Resources Engineering, Sustainable Process Engineering.ORCID iD: 0000-0003-1053-4623
Catalysis Research Unit, Department of Chemical Engineering, University of Cape Town.
Catalysis Research Unit, Department of Chemical Engineering, University of Cape Town.
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2004 (English)In: Recent advances in the science and technology of zeolites and related materials. Part A: proceedings of the 14th International Zeolite Conference, Amsterdam: Elsevier, 2004, p. 677-684Conference paper, Published paper (Refereed)
Abstract [en]

Alumina beads were coated with ZSM-5 films ranging from 150 nm to 2300 nm ill thickness. The ZSM-5 boated alumina beads were Subsequently hydrothermally treated in a silicalite-1 synthesis solution ill two steps Whereupon a dense silicalite-1 film was formed oil top of the ZSM-5 film. The materials were tested with two probe reactions and the reactivity was compared before and after coating with silicalite-1. As expected, the para-xylene (pX) isomerization reactivity showed no change for samples with and without the top layer of silicalite-1 for equal amounts Of zeolite. Surprisingly, the triisopropylbenzene (TIPB) conversion did not decrease after the silicalite-1 film was introduced. As measured by XPS, the aluminum concentration at the Surface of the uncalcined silicalite-1 film surface was lower compared to that at the Surface of the calcined ZSM-5 film. However, after calcination the concentration of aluminum was higher at the silicalite-1 film surface than at the ZSM-5 film Surface. These results Suggest that aluminum migrates from the ZSM-5 film into the silicalite-1 film during calcination and testing which results in all active top layer.

Place, publisher, year, edition, pages
Amsterdam: Elsevier, 2004. p. 677-684
National Category
Chemical Engineering
Research subject
Chemical Technology
Identifiers
URN: urn:nbn:se:ltu:diva-28463Scopus ID: 2-s2.0-11844256928Local ID: 245925f0-6f84-11db-962b-000ea68e967bISBN: 0-444-51827-4 (print)OAI: oai:DiVA.org:ltu-28463DiVA, id: diva2:1001660
Conference
International Zeolite Conference : 25/04/2004 - 30/04/2004
Note
Godkänd; 2004; 20060922 (bajo)Available from: 2016-09-30 Created: 2016-09-30 Last updated: 2025-02-18Bibliographically approved

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Öhrman, OlovHedlund, JonasSterte, Johan

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