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Material characterization of aluminum alloys for automotive and aerospace applications
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Solid Mechanics.ORCID iD: 0000-0002-8519-4937
2024 (English)Doctoral thesis, comprehensive summary (Other academic)
Abstract [en]

Aluminum alloys are one of the widely used materials in the structural components of automobiles and especially aircraft. The valid prediction of the performance and life span of these components via running simulations requires the usage of sophisticated physics-based material models. Such models are based on the mechanical response and the underlying microstructure evolution at varied deformation conditions. With the above motivation in mind, the aim of the current doctoral thesis was to investigate and understand the relationship between processing, microstructure, mechanical and fracture behavior of AA7075-T651 alloy and recycled AlSi10MnMg(Fe) alloy.

First, the deformation behavior of AA7075-T651 alloy, which was initially drawn from extruded round bars, was studied through compression tests at low (0.01 and 1 s−1) as well as at high (1400 – 5300 s−1) strain rates and deformation temperatures ranging between room temperature (RT) and 500 °C. At low strain rate deformation, the alloy experienced more softening due to adiabatic heating arising from 1 s−1 strain rate up to 200 °C. Beyond 200 °C, the softening effect was taken over by dynamic recovery and dynamic recrystallization which were enhanced by 0.01 s−1 strain rate. The deformation at high strain rates and elevated temperatures led to the formation of adiabatic shear bands (ASBs) and cracks in the material. The feasibility of formation and growth of ASBs and cracks increased with increase in strain and temperature, neglecting any significant effect from the strain rate.

Secondly, the recycled secondary AlSi10MnMg(Fe) alloy, which was produced by high pressure die casting (HPDC), was investigated. The secondary alloy showed great potential of exhibiting the strength and ductility within the range exerted by its conventional primary counterpart, i.e., AlSi10MnMg alloy, however, its tensile properties were restricted by the inhomogeneously formed fine-grained skin layer on the casting surface. The said inhomogeneity in skin formation was corresponded to the “waves and lakes” type of casting defect. Such inhomogeneous skin layer limited the ductility of the secondary alloy by undergoing abrupt fracture due to its poor bonding with the adjoining matrix. Even if the AlSi10MnMg(Fe) alloy used in the current research contained an abundance of porosity, cold flakes and intermetallics, which are known to be the driving factors behind the fracture of HPDC processed materials, the effect from the inhomogeneous skin was found out to be predominant.

Place, publisher, year, edition, pages
Luleå: Luleå University of Technology, 2024.
Series
Doctoral thesis / Luleå University of Technology, ISSN 1402-1544
Keywords [en]
AA7075, Recycled alloy, AlSi10MnMg(Fe) alloy, Dynamic recrystallization, Adiabatic shear bands, High pressure die casting, Inhomogeneous skin, Intermetallics
National Category
Metallurgy and Metallic Materials
Research subject
Solid Mechanics
Identifiers
URN: urn:nbn:se:ltu:diva-110123ISBN: 978-91-8048-644-6 (print)ISBN: 978-91-8048-645-3 (electronic)OAI: oai:DiVA.org:ltu-110123DiVA, id: diva2:1901057
Public defence
2024-11-22, E632, Luleå University of Technology, Luleå, 09:00 (English)
Opponent
Supervisors
Projects
ENABLEFlexcrash
Funder
EU, Horizon 2020, 764979EU, Horizon Europe, 101069674Available from: 2024-09-25 Created: 2024-09-25 Last updated: 2025-11-01Bibliographically approved
List of papers
1. Mechanical behavior and microstructure evolution during deformation of AA7075-T651
Open this publication in new window or tab >>Mechanical behavior and microstructure evolution during deformation of AA7075-T651
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2021 (English)In: Materials Science & Engineering: A, ISSN 0921-5093, E-ISSN 1873-4936, Vol. 822, article id 141615Article in journal (Refereed) Published
Abstract [en]

In view of developing a physics-based constitutive material model for AA7075-T651, the mechanical behavior and microstructure evolution of the material has been studied through compression tests using Gleeble thermo-mechanical simulator. The tests were performed at wide range of temperatures (room temperature (RT), 100, 200, 300, 400 and 500 °C) with two constant strain rates (0.01 and 1 s-1). The true stress-strain curves depicted an increase in the flow stress with increase in the strain rate and decrease in the deformation temperature, with an exception at RT. The effects of softening mechanisms, such as adiabatic heating, dissolution of precipitates, dynamic recovery (DRV) and dynamic recrystallisation (DRX), on the flow stress level, strain rate sensitivity (SRS) and temperature sensitivity over the entire range of temperatures were analyzed. Pertaining to the microstructure analysis, the intermetallic particles present in the initial as-received (AR) material were identified as (Al,Cu)6(Fe,Cu) and SiO2 with the help of back-scattered electron (BSE) imaging and energy dispersive X-ray spectroscopy (EDS). The microstructure of the material after the deformation processes were analyzed and compared with that of the AR state using inverse pole figures (IPF), grain orientation spread (GOS) and grain boundary rotation maps generated from electron back-scattered diffraction (EBSD) scans. DRV was observed for deformation at 300 °C, whereas a combination of DRV and incomplete DRX took place for 400 and 500 °C depending on the strain rate. The fraction of recrystallized grains was higher in case of deformation at higher temperature and lower strain rate. Furthermore, the difference in microstructure evolution on different surfaces of the deformed samples as well as at different locations on individual surfaces was also investigated.

Place, publisher, year, edition, pages
Elsevier, 2021
Keywords
Aluminum alloys, Characterization, Stress/strain measurements, Electron back-scattered diffraction (EBSD), Dynamic recrystallisation (DRX)
National Category
Metallurgy and Metallic Materials
Research subject
Solid Mechanics
Identifiers
urn:nbn:se:ltu:diva-84320 (URN)10.1016/j.msea.2021.141615 (DOI)000708189600003 ()2-s2.0-85108870288 (Scopus ID)
Note

Validerad;2021;Nivå 2;2021-08-11 (alebob);

Forskningsfinansiärer: European Union's Marie Skłodowska-Curie Actions (MSCA) Innovative Training Networks (ITN) H2020-MSCA-ITN-2017 (764979);

Full text license: CC BY;

For correction, see: Dalai, B., Moretti, M. A., Åkerström, P. et al. Corrigendum to “Mechanical behavior and microstructure evolution during deformation of AA7075-T651” [J. Mater. Sci. Eng. A 822 (2021) 141615]. Materials Science & Engineering: A, 845, 143210 (2022). https://doi.org/10.1016/j.msea.2022.143210

Available from: 2021-05-18 Created: 2021-05-18 Last updated: 2025-10-21Bibliographically approved
2. Mechanical behavior and microstructure evolution during high strain rate deformation of AA7075-T651
Open this publication in new window or tab >>Mechanical behavior and microstructure evolution during high strain rate deformation of AA7075-T651
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2022 (English)In: SN Applied Sciences, ISSN 2523-3963, E-ISSN 2523-3971, Vol. 4, no 10, article id 251Article in journal (Refereed) Published
Abstract [en]

The current study presents the effects of strain and temperature on the mechanical response and microstructure evolution in AA7075-T651 at high strain rates. Compression tests have been performed at room temperature (RT), 200, 300 and 400 °C using a Split-Hopkinson pressure bar (SHPB) setup with strain rates ranging between 1400 and 5300 s−1. For deformation at RT, the flow stress increases with increase in strain rate. Whereas deformation at elevated temperatures show a non-monotonous behavior of the flow stress with respect to the strain rate. This trait is attributed to the pronounced effects from the adiabatic shear bands (ASBs); namely, distorted shear bands (DSBs) and transformed shear bands (TSBs); and cracks resulting from the plastic deformation instability during hot deformation. The sequence of microstructure evolution is: inhomogeneity in the initial microstructure – DSB – TSB – crack –fracture. The feasibility of formation and growth of ASBs and cracks increases with increase in strain and temperature, neglecting any significant effect from the strain rate. During the compression tests, temperature of the material rises due to adiabatic heating. Considering a certain strain developed in the material, this adiabatic temperature rise decreases as the deformation temperature is increased. Furthermore, during individual deformation processes, the temperature rise increases with increasing strain. The adiabatic temperature leading to the formation of TSB is approximated to be 0.7 times of the melting temperature of the alloy. These results from the current study are to be used in developing a physics-based material model for the alloy.

Place, publisher, year, edition, pages
Springer, 2022
Keywords
AA7075-T651, Split-Hopkinson pressure bar, High strain rate, Stress/strain measurements, Optical microscopy, Adiabatic shear bands
National Category
Metallurgy and Metallic Materials
Research subject
Solid Mechanics
Identifiers
urn:nbn:se:ltu:diva-84323 (URN)10.1007/s42452-022-05141-6 (DOI)000849485700004 ()2-s2.0-85137553649 (Scopus ID)
Note

Validerad;2022;Nivå 2;2022-09-06 (johcin);

Funder: ENABLE project funded by the European Union’s Marie Skłodowska-Curie Actions (MSCA) Innovative Training Networks (ITN) H2020-MSCA-ITN-2017 under the Grant Agreement No 764979.;

This article has previously appeared as a manuscript in a thesis.

Available from: 2021-05-18 Created: 2021-05-18 Last updated: 2025-10-21Bibliographically approved
3. Inhomogeneous Skin Formation and Its Effect on the Tensile Behavior of a High Pressure Die Cast Recycled Secondary AlSi10MnMg(Fe) Alloy
Open this publication in new window or tab >>Inhomogeneous Skin Formation and Its Effect on the Tensile Behavior of a High Pressure Die Cast Recycled Secondary AlSi10MnMg(Fe) Alloy
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2025 (English)In: Metallurgical and Materials Transactions. A, ISSN 1073-5623, E-ISSN 1543-1940, Vol. 56, p. 196-218Article in journal (Refereed) Published
Abstract [en]

The current study investigated the microstructure evolution, mechanical properties, and fracture behavior of a high pressure die cast (HPDC) novel secondary alloy. The as-cast microstructure comprised (i) Primary α-Al, (ii) α-Al15(FeMn)3Si2 intermetallics, and (iii) Al–Si eutectics. The microstructure starting from the surface through the depth of the HPDC casting consisted of (i) fine-grained skin at surface, (ii) increased Al–Si eutectics at intermediate location, and (iii) coarse α-Al dendrites at center. Accordingly, the hardness increased from skin to the intermediate section and then decreased toward the center of the casting. The formation of skin layer was highly discontinuous, which was attributed to the complicated fluid flow pattern inside the die cavity. The skin layer indicated to slightly improve the strength of the HPDC alloy; however, it restricted the ductility of the material with a large variation. Such ductility behavior resulted from a fracture mechanism triggered by the inhomogeneous skin because of its poor bonding with the adjacent matrix. Even though the secondary alloy contained casting defects and α-Al15(FeMn)3Si2 intermetallics that are known to be driving factors for the fracture in such materials, the effects from the inhomogeneous skin turned out to be predominant in the current study. 

Place, publisher, year, edition, pages
Springer Nature, 2025
National Category
Metallurgy and Metallic Materials
Research subject
Solid Mechanics; Chemical Technology
Identifiers
urn:nbn:se:ltu:diva-110117 (URN)10.1007/s11661-024-07631-1 (DOI)001348684200003 ()2-s2.0-85208458511 (Scopus ID)
Projects
Flexcrash
Funder
EU, Horizon Europe, 101069674
Note

Validerad;2025;Nivå 2;2025-01-17 (joosat);

Full text license: CC BY

Available from: 2024-09-25 Created: 2024-09-25 Last updated: 2025-10-21Bibliographically approved
4. Evaluation of detrimental effect on the ductility caused by the inhomogeneous skin and casting defects in a high pressure die cast recycled secondary alloy
Open this publication in new window or tab >>Evaluation of detrimental effect on the ductility caused by the inhomogeneous skin and casting defects in a high pressure die cast recycled secondary alloy
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2025 (English)In: Materials Characterization, ISSN 1044-5803, E-ISSN 1873-4189, Vol. 221, article id 114775Article in journal (Refereed) Published
Abstract [en]

The usage of recycled alloys in the high pressure die casting (HPDC) applications for automobiles is gaining rapid interest. Even though the skin microstructure, which is typically induced on the casting surface during the HPDC process, is believed to improve the properties of the HPDC castings, it may not always form continuously throughout on the casting surface, and thereby can influence the mechanical properties. Thus, the current study evaluated and compared the effects of inhomogeneously formed surface skin with that of other defects on the ductility exhibited by the HPDC castings of a recycled secondary AlSi10MnMg(Fe) alloy. The formation of inhomogeneous skin in the current study was attributed to a phenomenon related to the “waves and lakes” type of defects created by the HPDC process. Such skin structure limited the ductility of the HPDC castings, irrespective of the tested strain rates in the current case, by undergoing abrupt fracture due to its poor bonding with the adjoining matrix resulting from the aforementioned inhomogeneity. Even if the investigated AlSi10MnMg(Fe) alloy contained an abundance of porosity, cold flakes and intermetallics, which are usually considered the driving factors behind the fracture of HPDC processed alloys, the effect from the inhomogeneous skin layer dominated all other factors in the current case. The order of detrimental effect on the ductility of HPDC processed AlSi10MnMg(Fe) alloy followed a sequence of inhomogeneous skin, cold flakes and pores, with the inhomogeneity in skin turning out to be the most harmful one.

Place, publisher, year, edition, pages
Elsevier, 2025
Keywords
Secondary alloy, AlSi10MnMg(Fe) alloy, High pressure die casting, Ductility, Inhomogeneous skin, Porosity, Cold flake
National Category
Materials Engineering
Research subject
Solid Mechanics; Experimental Mechanics; Chemical Technology
Identifiers
urn:nbn:se:ltu:diva-110120 (URN)10.1016/j.matchar.2025.114775 (DOI)001421696400001 ()2-s2.0-85216511859 (Scopus ID)
Projects
Flexcrash
Funder
EU, Horizon Europe, 101069674
Note

Validerad;2025;Nivå 2;2025-02-03 (signyg);

Full text license: CC BY

Available from: 2024-09-25 Created: 2024-09-25 Last updated: 2025-10-21Bibliographically approved

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