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A Modeling and Experimental Study of Microstructure Evolution and Mechanical Properties of Press Hardening Steels
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Solid Mechanics.ORCID iD: 0009-0008-4577-6626
2026 (English)Doctoral thesis, comprehensive summary (Other academic)
Abstract [en]

Within the automotive industry, the press hardening process has been increasingly used to manufacture components. The process allows for both ultra high strength as well as good design freedom of the components. The steel is first austenitized, followed by forming and cooling. The work within this thesis was aimed at modeling this process, where variations in the initial microstructure and austenitization parameters were introduced. The steel grade 22MnB5 was utilized throughout the work, with three different initial states being studied, hot rolled, cold rolled, and cold rolled which was soft annealed. Tensile testing was performed for rapidly quenched samples, as well as for samples cooled at lower rates, where mixtures of phases were present in the final microstructures. A phase transformation model was calibrated based on estimated final phase fractions, dilatometry, and EBSD reconstruction of the prior austenite. The effect of the austenitization parameters on grain growth was studied, where a grain growth model based on the average grain size and temperature was implemented. The relationship between the austenitization conditions and mechanical properties was evaluated with bending tests according to the standard VDA 238-100. To study the relationship between the microstructure evolution during cooling and the final tensile properties, 48 samples were heat treated with unique thermal histories. The temperature histories from the heat treatments were supplied to a phase transformation model, which in turn was coupled to a non-linear regression model that estimated the tensile properties. For a martensitic microstructure, there were minor differences in tensile properties for different initial states of the steel, with similar strength, ductility, and anisotropy. For lower cooling rates, the tensile properties and phase transformation kinetics displayed differences with respect to the initial steel. The grain growth was limited for samples heated up to 930 ˚C, and could be modeled based on the average grain size. For a higher austenitization temperature, there were instances of inhomogeneous grain growth. There were only minor effects of the austenitization conditions on the bending properties, with an average bending angle over 90 ˚C for all thermal histories. The estimations of the tensile properties displayed a minor effect of the split between the training and testing data, with an acceptable agreement with the measured properties. The work presented in this thesis can aid in the modeling of the press hardening process, giving insights into the effects of process variations.

Place, publisher, year, edition, pages
Luleå University of Technology, 2026.
Series
Doctoral thesis / Luleå University of Technology, ISSN 1402-1544
Keywords [en]
Press hardening, Hot stamping, 22MnB5, Phase transformation modeling, Automotive steels
National Category
Solid and Structural Mechanics
Research subject
Solid Mechanics
Identifiers
URN: urn:nbn:se:ltu:diva-117558ISBN: 978-91-8142-079-1 (print)ISBN: 978-91-8142-080-7 (electronic)OAI: oai:DiVA.org:ltu-117558DiVA, id: diva2:2061311
Public defence
2026-09-04, E231, Luleå University of Technology, Luleå, 09:00 (English)
Opponent
Supervisors
Available from: 2026-05-21 Created: 2026-05-20 Last updated: 2026-08-14Bibliographically approved
List of papers
1. Investigating the Tensile Properties of 22MnB5 After Austenitization and Quenching with Different Initial Microstructures
Open this publication in new window or tab >>Investigating the Tensile Properties of 22MnB5 After Austenitization and Quenching with Different Initial Microstructures
2025 (English)In: Metals, E-ISSN 2075-4701, Vol. 15, no 6, article id 589Article in journal (Refereed) Published
Abstract [en]

In the automotive industry, structural components are often produced via press hardening, enabling rapid production and the use of ultra-high-strength steels. In this process, steels are heated to an austenitic state and are then formed and quenched in rapid succession. The initial steel that enters the press-hardening production line varies, where the microstructure is a result of previous production steps. This work was performed to investigate the possible effects of the initial microstructure on the final mechanical properties for rapidly quenched samples. Although the initial microstructure is transformed during austenitization, the steel can still be affected by its prior history. Steels with three different initial microstructures were evaluated, with only minor variations in chemical composition and thicknesses. The Lankford coefficients and the failure strains were dependent on the orientation of the samples. However, for a given orientation, there were only minor variations between the different steels with respect to anisotropy, strength, and ductility. The anisotropy could be correlated with the microstructure through the calculation of Taylor factors based on measurements using electron backscatter diffraction. The minor influence from the initial steel microstructure on the final mechanical properties indicates robustness suitable for mass production.

Place, publisher, year, edition, pages
MDPI, 2025
Keywords
press hardening, hot stamping, 22MnB5, Lankford coefficients, anisotropy
National Category
Metallurgy and Metallic Materials
Research subject
Solid Mechanics
Identifiers
urn:nbn:se:ltu:diva-113992 (URN)10.3390/met15060589 (DOI)001516030300001 ()2-s2.0-105009024154 (Scopus ID)
Funder
Luleå University of Technology
Note

Validerad;2025;Nivå 2;2025 (u5);

Full text license: CC BY 4.0; 

Funder: Gestamp Hardtech AB;

Available from: 2025-07-03 Created: 2025-07-03 Last updated: 2026-05-20Bibliographically approved
2. The Influence of Austenitization Conditions on Grain Growth and the Bending Performance of Boron Steel
Open this publication in new window or tab >>The Influence of Austenitization Conditions on Grain Growth and the Bending Performance of Boron Steel
2026 (English)In: Metallurgical and materials transactions. B, process metallurgy and materials processing science, ISSN 1073-5615, E-ISSN 1543-1916, Vol. 57B, no 1, p. 552-563Article in journal (Refereed) Published
Abstract [en]

During production of components using press hardening, the steel will at one point be heated to an austenitic state. Grain growth can occur during this austenitization if the time and temperature are sufficient, where the microstructure becomes increasingly coarse. The final austenite grain size can affect both the phase transformations during quenching and the final mechanical properties of a fully martensitic microstructure. In this work, austenite grain growth was modeled using measurements of the mean grain diameters from isothermal experiments, while the model was validated using non-isothermal experiments. The temperature and time ranges used in the isothermal experiments were 900–960 C and 1-1200 seconds, respectively. Bending tests according to VDA 238-100 were performed, using samples previously austenitized at 900, 930, and 960 C and then rapidly quenched. The isothermal grain growth up to 930 C could be modeled using the average grain size, while at 960 C the microstructure displayed a more complex growth behavior. The grain growth during the non-isothermal validation experiments could be predicted with the exception of one thermal cycle. No effect of the austenitization temperature on the bending performance was observed when short austenitization times were utilized, and only a minor effect was observed for a longer austenitization time.

Place, publisher, year, edition, pages
Springer Nature, 2026
National Category
Metallurgy and Metallic Materials
Research subject
Solid Mechanics; Engineering Materials
Identifiers
urn:nbn:se:ltu:diva-115744 (URN)10.1007/s11663-025-03814-2 (DOI)001621568900001 ()2-s2.0-105022834700 (Scopus ID)
Projects
PROCHAIN
Note

Full text license: CC BY 4.0;

Funder: Gestamp Hardtech AB

Available from: 2025-12-10 Created: 2025-12-10 Last updated: 2026-06-30Bibliographically approved
3. Phase transformation kinetics and its variability due to initial microstructure - a numerical and experimental study for the steel 22MnB5
Open this publication in new window or tab >>Phase transformation kinetics and its variability due to initial microstructure - a numerical and experimental study for the steel 22MnB5
(English)Manuscript (preprint) (Other academic)
National Category
Solid and Structural Mechanics
Research subject
Solid Mechanics
Identifiers
urn:nbn:se:ltu:diva-117556 (URN)
Available from: 2026-05-20 Created: 2026-05-20 Last updated: 2026-06-03Bibliographically approved
4. Estimation of tensile properties of a press hardenable steel subjected to complex cooling paths
Open this publication in new window or tab >>Estimation of tensile properties of a press hardenable steel subjected to complex cooling paths
(English)Manuscript (preprint) (Other academic)
National Category
Solid and Structural Mechanics
Research subject
Solid Mechanics
Identifiers
urn:nbn:se:ltu:diva-117557 (URN)
Available from: 2026-05-20 Created: 2026-05-20 Last updated: 2026-05-28Bibliographically approved

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Lundholm, Erik

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